复合材料中有机化合物的释放取决于固化光源、浸泡溶液和PH值

Karina Alessandra Michelão Grecca Pieroni, Alexandra Mussolino Queiroz, Marília Pacífico Lucisano
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摘要

目的:采用荧光光谱法,通过不同的固化光源、不同的浸泡溶液和不同的pH值,研究了复合KaloreTM (GC FUJI)和FiltekTM Silorane (3M ESPE)对有机化合物的体外释放。方法:每种复合材料制备56个标本,卤素光聚合28个,LED光聚合28个。每种复合材料的样品分别保存在pH值为中性或酸性的水中和pH值为酸性或中性的唾液中(每种检查条件n=7个样品)。读数在1 - 672小时(28天)之间进行。统计分析采用Tukey检验和ANOVA检验,显著性水平为5%。结果:在卤素光聚合和LED光聚合两种ph值下,KaloreTM树脂在水环境下比FiltekTMSilorane树脂释放出更多的有机化合物(p0.05)。在人工唾液中,KaloreTM树脂也比FiltekTMSilorane树脂释放出更多的有机化合物,但在中性pH和酸性pH下,在LED光下聚合时,两者之间的差异只有统计学意义。无论光源和pH如何,两种树脂在水溶液中释放的有机化合物量都高于唾液(p<0.05)。结论:即使是最现代的树脂如KaloreTM和FiltekTM硅烷也会释放有机化合物,LED光聚合降低了FiltekTM硅烷树脂对有机化合物的释放。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Release of Organic Compounds by Composites Depending on the Source of Curing Light, Immersion Solution and PH
Objectives: This in vitro study evaluated the release of organic compounds by composite KaloreTM (GC FUJI) and FiltekTM Silorane (3M ESPE) by means of fluorescence spectrometry, varying the source of curing light, the immersion solution and the pH of these immersions. Methods: 56 specimens were made for each composite, 28 polymerized with halogen light and 28 with LED light. Samples of each composite were stored in water with neutral or acidic pH and in saliva with acidic or neutral pH (n=7 specimens for each condition examined). The reading was performed between 1 and 672 hours (28 days).The results were statistically analyzed using the Tukey and ANOVA tests, adopting the significance level of 5%. Results: The KaloreTM resin released more organic compounds than FiltekTMSilorane in the aqueous environment, either in the polymerization by the halogen light as by the LED light in both pHs (p<0.05). There was no significant difference in aqueous environment, only when polymerized by halogen light and acid pH (p>0.05). When immersed in artificial saliva, the KaloreTM resin also released more organic compounds than FiltekTMSilorane, but there was only statistically significant difference when polymerized by LED light, both in neutral pH and at acid pH. Both resins released greater amount of organic compounds in aqueous solution, compared to saliva, regardless of the light source and pH (p<0.05). Conclusion: Even the most modern resins such as KaloreTM and FiltekTM Silorane release organic compounds and the polymerization by LED light decreases the liberation of organic compounds by FiltekTM Silorane resin.
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