热等离子体中用于纳米粒子合成的原料粒子动力学成像激光频闪测量

R. Furukawa, K. Akashi, Y. Nagase, Yasunori Tanaka, Y. Nakano, T. Ishijima, S. Sueyasu, Shu Watanabe, K. Nakamura
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引用次数: 0

摘要

纳米颗粒是尺寸为100纳米或更小的颗粒,具有与块状材料不同的特性。对于纳米颗粒的各种应用,需要开发一种高速率的纳米颗粒合成方法。作者已经开发了脉冲调制感应热等离子体(PMITP)和时间控制进料(TCFF)方法,作为合成大量纳米颗粒的方法[1]。在PMITP中,通过对矩形波形的高频线圈电流进行调幅,可以将热等离子体的温度控制在毫秒级。在该PMITP中,原料颗粒被间歇注入,在高温期蒸发,蒸发后的原料蒸汽被输送到等离子炬下游,在那里由于过饱和状态发生成核,生成纳米颗粒。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Imaging of Feedstock Particle Dynamics in Thermal Plasma for Nanoparticle Sythesis by Laser-Strobe Measurement
Nanoparticles are particles with a size of 100 nm or less, which have different properties from bulk materials. For various applications of such nanoparticles, it is desired to develop a high-rate synthesis method for nanoparticles. The authors have developed pulse modulated induction thermal plasma (PMITP) and time-controlled feedstock feeding (TCFF) method, as a method for synthesizing large amounts of nanoparticles [1]. In PMITP, the temperature of thermal plasma can be controlled in the order of milliseconds by amplitude-modulating the high-frequency coil current in a rectangular waveform. To this PMITP, feedstock particles are intermittently injected to be evaporated in high-temperature period, and then the evaporated feedstock vapor is transported to downstream of the plasma torch, where nucleation occurs due to supersaturation state, generating nanoparticles.
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