纳米颗粒 TiO2:利用R.F.磁控溅射技术在不锈钢316L上镀银薄膜,用于模拟体液(SBF)中的防腐

Wahraan Mohammed Hussein, Abdulhussein K. Elttayef, S. Khalil
{"title":"纳米颗粒 TiO2:利用R.F.磁控溅射技术在不锈钢316L上镀银薄膜,用于模拟体液(SBF)中的防腐","authors":"Wahraan Mohammed Hussein, Abdulhussein K. Elttayef, S. Khalil","doi":"10.1063/1.5138565","DOIUrl":null,"url":null,"abstract":"In this research, TiO2 nanoparticles were prepared using the Sol-Gel method and mixed with different addition concentration of (3,5and7)% ww Ag nanoparticles for TiO2: Ag and obtained different thickness on the base used (Stainless 316L). These films were placed in an oven (600 ° C) for one hour to improve the crystallization structure of thin films. The AFM, SEM, EDX and XRD inspections revealed useful data on particle size, shape, surface elemental, and the structure. (AFM,SEM, X- ray, EDS) tested and showed that the minimum particle size was (35 nm) for TiO2: Ag at 7% of silver and corrosion in stainless steel in SBL using the electrochemical method (Tafel curves). All samples achieved excellent results to reduce corrosion but at different rates was the best result TiO2:Ag 3%","PeriodicalId":186251,"journal":{"name":"TECHNOLOGIES AND MATERIALS FOR RENEWABLE ENERGY, ENVIRONMENT AND SUSTAINABILITY: TMREES19Gr","volume":"26 3 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2019-12-11","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"Nanoparticles TiO2: Ag thin films coated stainless steel 316L by R.F. magnetron sputtering technique for anticorrosion in simulated body fluid (SBF)\",\"authors\":\"Wahraan Mohammed Hussein, Abdulhussein K. Elttayef, S. Khalil\",\"doi\":\"10.1063/1.5138565\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"In this research, TiO2 nanoparticles were prepared using the Sol-Gel method and mixed with different addition concentration of (3,5and7)% ww Ag nanoparticles for TiO2: Ag and obtained different thickness on the base used (Stainless 316L). These films were placed in an oven (600 ° C) for one hour to improve the crystallization structure of thin films. The AFM, SEM, EDX and XRD inspections revealed useful data on particle size, shape, surface elemental, and the structure. (AFM,SEM, X- ray, EDS) tested and showed that the minimum particle size was (35 nm) for TiO2: Ag at 7% of silver and corrosion in stainless steel in SBL using the electrochemical method (Tafel curves). All samples achieved excellent results to reduce corrosion but at different rates was the best result TiO2:Ag 3%\",\"PeriodicalId\":186251,\"journal\":{\"name\":\"TECHNOLOGIES AND MATERIALS FOR RENEWABLE ENERGY, ENVIRONMENT AND SUSTAINABILITY: TMREES19Gr\",\"volume\":\"26 3 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2019-12-11\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"TECHNOLOGIES AND MATERIALS FOR RENEWABLE ENERGY, ENVIRONMENT AND SUSTAINABILITY: TMREES19Gr\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.1063/1.5138565\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"TECHNOLOGIES AND MATERIALS FOR RENEWABLE ENERGY, ENVIRONMENT AND SUSTAINABILITY: TMREES19Gr","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1063/1.5138565","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 2

摘要

本研究采用溶胶-凝胶法制备TiO2纳米粒子,并在基体(不锈钢316L)上加入不同浓度的(3、5、7)% ww Ag纳米粒子混合制备TiO2: Ag,得到不同厚度的纳米粒子。这些薄膜被放置在烤箱(600°C) 1小时,以改善薄膜的结晶结构。AFM, SEM, EDX和XRD检测显示了颗粒大小,形状,表面元素和结构的有用数据。(AFM,SEM, X射线,EDS)测试表明,在银含量为7%时,TiO2: Ag的最小粒径为(35 nm),并且在SBL中对不锈钢的腐蚀(Tafel曲线)。所有样品都取得了优异的减腐蚀效果,但在不同的速率下,TiO2:Ag 3%的效果最好
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Nanoparticles TiO2: Ag thin films coated stainless steel 316L by R.F. magnetron sputtering technique for anticorrosion in simulated body fluid (SBF)
In this research, TiO2 nanoparticles were prepared using the Sol-Gel method and mixed with different addition concentration of (3,5and7)% ww Ag nanoparticles for TiO2: Ag and obtained different thickness on the base used (Stainless 316L). These films were placed in an oven (600 ° C) for one hour to improve the crystallization structure of thin films. The AFM, SEM, EDX and XRD inspections revealed useful data on particle size, shape, surface elemental, and the structure. (AFM,SEM, X- ray, EDS) tested and showed that the minimum particle size was (35 nm) for TiO2: Ag at 7% of silver and corrosion in stainless steel in SBL using the electrochemical method (Tafel curves). All samples achieved excellent results to reduce corrosion but at different rates was the best result TiO2:Ag 3%
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信