溶胶-凝胶喷涂法在玻璃基板上沉积TiO2, ZnO, TiO2: ZnO薄膜及其在染料降解中的应用

Wilda Amananti, Wilda Amananti
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引用次数: 0

摘要

采用喷涂技术的溶胶-凝胶法在玻璃基板上沉积了TiO2、ZnO和TiO2: ZnO薄膜。TiO2: ZnO和ZnO可以在玻璃衬底上形成。采用喷涂技术的溶胶-凝胶法制备了TiO2和TiO2: ZnO的前驱体溶液。将脱水乙酸锌(Zn (COOCH3) 2.2 h2o)溶于异丙醇((CH3) 2CHOH)溶剂中,加入单乙醇胺(MEA: HOCH2CH2NH2),在70℃下搅拌,得到清澈均匀的溶液。四异丙醇钛(TTIP) 0.73 ml溶于4.27 ml异丙醇和20 ml乙醇中,用5 ml乙醇、3.4 ml乙酸和0.26 ml H2O滴定,室温下用热板搅拌器搅拌(进一步将ZnO、TiO2和TiO2:将ZnO前驱体凝胶喷射在450℃加热的玻璃基板上,测量TiO2薄膜带隙能量为3.58 eV, ZnO薄膜为3.08 eV, TiO2薄膜为3.06 eV,在紫外反应器中掺杂光降解染料直蓝10 ppm, TiO2: ZnO薄膜的降解率最高
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Analysis of Optical Properties TiO2, ZnO, TiO2: ZnO Thin Films Deposited On Glass Substrate Using Sol-Gel Spray Coating Method And Application For Degradation Of Dye Liquids.
TiO2, ZnO and TiO2: ZnO Thin film have been deposited on glass substrate by sol-gel method of Spray Coating Technique. TiO2: ZnO and ZnO can form well above the glass substrate. The precursor solution of TiO2 and TiO2: ZnO is deposited using sol-gel method of Spray Coating Technique. Zinc acetate dehydrate (Zn (COOCH3) 2 .2H2O was dissolved into an isopropanol ((CH3) 2CHOH) solvent and then added monoethanolamine (MEA: HOCH2CH2NH2) .The solution was stirred at 70oC until a clear and homogeneous solution was obtained.Titanium Tetraisopropoxide (TTIP) 0 , 73 ml was dissolved into 4.27 ml of isopropanol and 20 ml of ethanol, after which the solution was titrated with 5 ml of ethanol, 3.4 ml acetic acid and 0.26 ml H2O, then stirred on hot plate stirrer at room temperature ( Further, the ZnO, TiO2 and TiO2: ZnO precursor gels were sprayed on a glass substrate that was heated at a temperature of 450 ° C. The results of the TiO2 thin film bandgap energy measurement were 3.58 eV, ZnO thin films of 3.08 eV, and a thin layer of TiO2: ZnO of 3.06 eV Doped photodegradation dye Direct blue 10 ppm using UV-reactor The highest percentage of degradation is found in TiO2: ZnO thin film
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