一种由MgB2/不锈钢制成的零电阻导线,通过冷面对机械特征和微结构的修正形状进行了改装

Satrio Herbirowo, Andika Widya Pramono
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引用次数: 1

摘要

二硼化镁(MgB2)是一种具有零电阻和高效率的医疗和电气应用的高电位材料。将纯度为98%的Mg粉末和纯度为95%的B非晶态原料按1:2的比例混合,用玛玛石砂浆研磨2小时,压实后用管中粉(PIT)插入不锈钢(SS)管中。SS管先前在900°C下退火1小时。采用马弗炉在800℃温度下烧结1小时,然后进行冷轧线材逐渐还原。采用维氏显微硬度计和极限拉伸试验机对试样的力学性能进行了表征。用光学显微镜观察了样品的表面形貌,用SEM-EDAX仪测量了样品的超导性能。在尺寸减小60%的情况下,达到了最高的硬度值377,2 HV,抗拉强度为1381 KN/mm。形貌观察结果表明,合金变形均匀,无裂纹,晶粒形态趋于结晶。在临界温度为39.55K时,MgB2丝的超导性降低了40%,出现了零电阻现象
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Fabrikasi Kawat Resistansi Nol Berbahan MgB2/Stainless Steel dengan Variasi Reduksi Ukuran melalui Pengerolan Dingin terhadap Karakteristik Mekanik dan Struktur Mikro
Magnesium Diboride (MgB2) is a high potential material for medical and electrical applications with zero resistance and high efficiency. The raw materials of Mg powder with a purity of 98% and B amorphous with a purity of 95%, were mixed with a ratio of 1:2, ground for 2 hours using an agate mortar, and subsequently compacted and inserted into stainelss steel (SS) tube by powder-in-tube (PIT). The SS tube was previously annealed at 900°C for 1 hour. The sintering process was carried out using a muffle furnace at a temperature of 800°C for 1 hour, followed by cold wire rolling with gradual reduction. The samples were characterized  for their mechanical properties using Vickers microhardness tester and ultimate tensile test machine. Surface morphologies of samples were observed using optical microscope and SEM-EDAX Superconducting properties were measured with the cryogenic resistance measurement. The highest hardness value of 377,2 HV was achieved at a 60% size reduction along with the tensile strength of 1381 KN/mm. The results of the morphological observation showed homogeneous deformation without any cracks, with the the grain shape tended to be crystalline. The superconductivity test showed the phenomenon of zero resistance at a critical temperature of 39.55K at a 40% reduction in MgB2 wire
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