柠檬酸稳定银纳米粒子:晶体学和表面性质的研究

Nabraj Bhattarai, S. Khanal, P. R. Pudasaini, Shanna Pahl, Dulce Romero-Urbina
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引用次数: 16

摘要

合成了柠檬酸稳定银(Ag)胶体溶液,并利用透射电子显微镜(TEM)和zeta电位测量技术对其晶体学和表面性质进行了表征。TEM研究表明,Ag的粒径在5 ~ 50 nm之间,较小的颗粒具有单晶结构,较大的颗粒具有结构缺陷(如多重孪晶、高聚结和云纹图案)。ζ电位测定证实了Ag +在nAg原液中的存在。过滤后的溶液中,ζ电位的位移为+25.1 mV,表明Ag - o纳米颗粒中存在Ag +。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Citrate Stabilized Silver Nanoparticles: Study of Crystallography and Surface Properties
Citrate stabilized silver (Ag) colloidal solution were synthesized and characterized for crystallographic and surface properties by using transmission electron microscopy (TEM) and zeta potential measurement techniques. TEM investigation depicted the size of Ag o ranges from 5 to 50 nm with smaller particles having single crystal structure while larger particles with structural defects (such as multiply twinned, high coalescence and Moire patterns). ζ-potential measurement confirms the presence of Ag + in nAg stock solution. The shift in ζ-potential measurement by +25.1 mV in the filtered solution suggests the presence of Ag + in Ag o nanoparticles.
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