紫外-可见光谱法分析了浓度对吸光度的影响

Jamal Moammar Aldabib, M. Edbeib
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引用次数: 2

摘要

这个实验利用了被称为紫外可见光谱的材料表征技术。本研究的目的是研究紫外可见吸收光谱读数,以研究浓度对金溶液吸光度的影响,并确定粉末样品(tio2)的带隙值。二氧化钛样品的类型可以表征为粉末的固体形式、薄膜和/或液体形式。不同状态试样的制备方法是不同的。本研究利用紫外-可见光谱技术对分散在不同浓度乙醇中的金纳米颗粒液体样品进行了表征。样品的吸光度-浓度曲线符合比尔定律。当以二氧化钛粉末的形式检测固体状态时,在进行实验之前需要对样品进行包装。为了从紫外-可见光谱的反射数据计算出各物质的带隙,绘制了能量(eV)与带隙的关系图。快速识别j曲线,外推切线与x轴相交,得到带隙值。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The effects of concentration based on the absorbance form the ultraviolet–visible (UV-VIS) spectroscopy analysis
This experiment utilizes the material characterization technique known as UV-Vis spectroscopy. The aim of this research is to study the UV-Vis absorption spectroscopy readout in order to investigate the effect of concentration on absorbance for gold solution and to determine the value of band gap for powder sample (TiO 2 ). The types of TiO 2 specimens can be characterized on a solid form of powder, thin film and/or in a liquid form. The preparation of each state of specimen are varies. In this current research, Liquid samples of Au nanoparticles dispersed in different concentrations of ethanol were characterized using UV-Vis technique. The absorbance versus concentration plot of the Au-ethanol samples were found to obey Beer’s law. When examining the solid state in a form of TiO 2 powder, the sample need to be packed before running the experiment. To calculate the band gap of each matter from the reflectance data of UV-Vis, the graph of energy (eV) versus is plotted. The J-curve is identified quickly, extrapolating the tangent to intersect the x-axis to obtain the band gap value.
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