不同电位条件下电浆法制备氧化铝涂层的研究

M. Amiri, S. Padervand, Vahid Tavakoli Targhi, S. M. M. Khoei
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引用次数: 5

摘要

铝表面镀膜的重要方法之一是电解等离子体镀膜法。本研究的主要目的是探讨电解等离子体法制备氧化铝涂层的潜力。采用铝系2和硅酸钠、四磷酸钠、铝酸钠和氢氧化钾作为电解液。结果表明,达到理想镀层厚度和形貌的最佳电压为500 V。在电解质溶液中加入硅酸钠会产生多孔性和不粘附在基材上。另一方面,四焦磷酸钠的使用通过将磷渗透到金属/涂层界面来增加涂层的附着力。等离子体电解氧化涂层的最佳溶液分别为10、3、3 g/l的四焦磷酸钠、铝酸钠和KOH。结果表明,直流脉冲涂层可以控制涂层过程和涂层均匀性。此外,在30%占空比下,应用直流脉冲电位覆盖的适当频率为1000hz。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Investigation of aluminum oxide coatings created by electrolytic plasma method in different potential regimes
One of the most important coating methods on aluminum surfaces is the electrolytic plasma method. The main objective of the present study is to investigate the potential of aluminum oxide coatings created by electrolytic plasma method. Aluminum series 2 and the electrolyte of sodium silicate, sodium tetraphosphate, sodium aluminate and potassium hydroxide were used. The results showed that the appropriate voltage to achieve uniform coating with ideal thickness and morphology is 500 V. Adding sodium silicate to the electrolyte solution will create porosity and non-adhesion to the substrate. On the other hand, the use of tetra sodium pyrophosphate increases the adhesion of the coating by penetrating phosphorus into the metal/coating interface. The optimum solution for plasma electrolytic oxidation coatings composed of 10, 3, and 3 g/l of tetra sodium pyrophosphate, sodium aluminate and KOH, respectively. DC pulsed coating was shown to control the coating process and coating uniformity. Also the appropriate frequency for coverage with the applied DC pulse potential is 1000 Hz under the 30% duty cycle.
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