斜面跟踪(IPT)试验分析硅橡胶固化特性及泄漏电流特性

N. N. Ali, H. Zainuddin, J. A. Razak, R. Abd-Rahman
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引用次数: 2

摘要

为了探索硅橡胶(SiR)材料独特的绝缘性能,世界各地仍在进行研究。因此,本研究旨在进一步分析不同填料含量对SiR配方的影响、固化特性及其对样品电性能的影响。首先,将三种不同浓度的三水合氧化铝(ATH) (10wt%, 20wt%和30wt%)与过氧化二氨基(DCP)作为固化剂配制成SiR。根据ASTM D5289使用流变仪测试了三种不同浓度SiR的固化特性。然后根据BSEN 60587斜面跟踪(IPT)测试标准对制备的SiR材料进行测试,通过泄漏电流(LC)值分析其电气性能。结果表明,填料用量增加,交联密度(MH)增加,焦化时间(TS2)缩短。固化时间随着填料量的增加而增加。填充量增加至30wt%,再加上交联密度(MH),使SiR材料具有良好的电性能。当ATH添加量为30wt%时,交联密度最高,焦化时间最短,固化时间最长,LC值最低,为9.7 mA。总体而言,适当的ATH填料负载的组合有助于高交联密度和更高的样品抗跟踪和侵蚀阻力,因此LC值较低。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Curing Characteristic Analysis and Leakage Current Performances of Silicone Rubber via Inclined Plane Tracking (IPT) Test
Researches are still being performed all around the world in order to explore the unique insulating behavior of Silicone Rubber (SiR) material. Hence, this research is performed in order to analyze more on the effect of SiR formulation with different filler content, their curing characteristic and their effect upon sample performances electrically. Firstly, SiR will be formulated with three different concentration of Alumina Trihydrate (ATH) of 10wt%, 20wt% and 30wt% together with Dicumyl peroxide (DCP) as the curing agent. The cure characteristic of the SiR with all three different concentrations were tested using rheometer in accordance to ASTM D5289. The prepared SiR materials were then tested according to the standard of BSEN 60587 Inclined Plane Tracking (IPT) test in order to analyze their performances electrically via leakage current (LC) values. It was found that increase in filler loadings were followed by increase in crosslinking density (MH) and decrease in scorch time (TS2). The cure time increases with increase in filler loadings. The increase in filler loading up to 30wt% together with crosslinking density (MH) have contributed towards a SiR material with great electrical properties. The highest ATH loadings of 30wt% displayed the highest crosslinking density, lowest scorch time, highest cure time and lowest LC value of 9.7 mA. In overall, a combination of proper ATH filler loading contributes to a high crosslinking density and higher resistance of sample against tracking and erosion and hence a lower LC value.
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