改性Hummer法合成“间竹”基氧化石墨烯晶体结构分析

Ledia Elan Safitri, Ramli, Gusnedi, R. Hidayat
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摘要

竹子是一种非用材林产品,在印度尼西亚有非常多的人口。其中之一是竹子,从低地到高地都可以找到,但没有得到适当的利用。因此,进行了利用竹子造福社会的研究。在本研究中,将以竹材为原料合成氧化石墨烯(GO)。合成氧化石墨烯的目的是进一步观察氧化石墨烯本身的晶体结构和晶体尺寸,因为氧化石墨烯可以应用于各种领域,如吸波器、射频电子、数据显示板、光伏电池等。采用改进的Hummers法合成氧化石墨烯。本研究采用的烧结温度分别为300℃、350℃、400℃和4500C。利用XRD和FTIR对氧化石墨烯进行表征,揭示了氧化石墨烯的晶体体系、晶体结构和尺寸、附加官能团和物相。氧化石墨烯的平均晶粒尺寸为23.30165 nm,是最大的平均晶粒尺寸。氧化石墨烯层是由碳(C)、氢(H)和氧(O)之间的键合形成的,在任何温度变化下都可以形成氧化石墨烯层。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Crystal Structure Analysis of Graphene Oxide based on Bamboo “Betung” Synthesized By Modi-Fied Hummer Method
Bamboo is a non-timber forest product with a very large population in Indonesia. One of them is bamboo betung which can be found from the lowlands to the highlands but has not been used properly. Therefore, research was conducted to utilize bamboo betung to benefit the society. In this study, the synthesis of graphene oxide (GO) from bamboo betung stems will be carried out. The purpose of  GO synthesis to further observe the crystal structure and crystal size of GO itself because it can be applied in various fields such as wave absorbers, radio frequency electronics, data display panels, and photovoltaic cells. GO synthesis was carried out using the Modified Hummers Method. The sintering temperatures used in this study were 300oC, 350oC, 400oC and 4500C. GO characterization was carried out using XRD and FTIR to reveal the system of crystal, crystal structure, and size, in addition functional groups, and phases of graphene oxide. GO has an average crystal size of 23.30165 nm as the largest average crystal size. GO layer is formed due to the bond between Carbon (C), Hydrogen (H) and Oxygen (O). GO Layer can be typed at any temperature variations carried out..
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