Alaa F. Hashim Al- Ajeeli, Khalid. H. Razeg, Ibrahim Fuad Tariq
{"title":"用溶胶-凝胶化学方法研究二氧化硅核壳纳米铜作为抗菌剂","authors":"Alaa F. Hashim Al- Ajeeli, Khalid. H. Razeg, Ibrahim Fuad Tariq","doi":"10.17993/3ctecno.2023.v12n1e43.337-352","DOIUrl":null,"url":null,"abstract":"Core-shell Cu@sio2 nanoparticles were created by a chemical reaction in a sol gel, and their ability to inhibit S. aureus and E. coli bacteria was tested, when synthesized and characterized using ultraviolet-visible spectroscopy, a copper band could be seen before and after encapsulation at wavelengths of 625 nanometers and 635 nanometers, which are surface plasmonic resonant frequency bands, respectively. The production of Cu @Sio2 core shell nanoparticles was further confirmed using field emission scanning electron microscope (FESEM) pictures. The core shell nanoparticles have a mean size of 66 nanometers and a spherical shape, as shown in TEM. The X-ray diffraction patterns for the nanoparticles, which show face-centered cubic (FCC) of copper, match the crystal structure of Cu@sio2 we discovered using fourier transform infrared (FT-IR) spectroscopy, the fourier transform infrared interaction between the silica and the synthesized copper NPs was investigated. This revealed the capping of the CuNPs by SiO2. The inhibition zone was evident as a result of the activities of these compounds (14, 14, 16, and 20) and (24, 24, 28, and 30) against Escherichia coli bacteria and Staphylococcus aureus bacteria, respectively.","PeriodicalId":210685,"journal":{"name":"3C Tecnología_Glosas de innovación aplicadas a la pyme","volume":"37 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-03-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Copper At Silica Core - Shell Nanoparticles As Antibacterial Agents By Sol-Gel Chemical Methods\",\"authors\":\"Alaa F. Hashim Al- Ajeeli, Khalid. H. Razeg, Ibrahim Fuad Tariq\",\"doi\":\"10.17993/3ctecno.2023.v12n1e43.337-352\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Core-shell Cu@sio2 nanoparticles were created by a chemical reaction in a sol gel, and their ability to inhibit S. aureus and E. coli bacteria was tested, when synthesized and characterized using ultraviolet-visible spectroscopy, a copper band could be seen before and after encapsulation at wavelengths of 625 nanometers and 635 nanometers, which are surface plasmonic resonant frequency bands, respectively. The production of Cu @Sio2 core shell nanoparticles was further confirmed using field emission scanning electron microscope (FESEM) pictures. The core shell nanoparticles have a mean size of 66 nanometers and a spherical shape, as shown in TEM. The X-ray diffraction patterns for the nanoparticles, which show face-centered cubic (FCC) of copper, match the crystal structure of Cu@sio2 we discovered using fourier transform infrared (FT-IR) spectroscopy, the fourier transform infrared interaction between the silica and the synthesized copper NPs was investigated. This revealed the capping of the CuNPs by SiO2. The inhibition zone was evident as a result of the activities of these compounds (14, 14, 16, and 20) and (24, 24, 28, and 30) against Escherichia coli bacteria and Staphylococcus aureus bacteria, respectively.\",\"PeriodicalId\":210685,\"journal\":{\"name\":\"3C Tecnología_Glosas de innovación aplicadas a la pyme\",\"volume\":\"37 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-03-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"3C Tecnología_Glosas de innovación aplicadas a la pyme\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.17993/3ctecno.2023.v12n1e43.337-352\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"3C Tecnología_Glosas de innovación aplicadas a la pyme","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.17993/3ctecno.2023.v12n1e43.337-352","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Copper At Silica Core - Shell Nanoparticles As Antibacterial Agents By Sol-Gel Chemical Methods
Core-shell Cu@sio2 nanoparticles were created by a chemical reaction in a sol gel, and their ability to inhibit S. aureus and E. coli bacteria was tested, when synthesized and characterized using ultraviolet-visible spectroscopy, a copper band could be seen before and after encapsulation at wavelengths of 625 nanometers and 635 nanometers, which are surface plasmonic resonant frequency bands, respectively. The production of Cu @Sio2 core shell nanoparticles was further confirmed using field emission scanning electron microscope (FESEM) pictures. The core shell nanoparticles have a mean size of 66 nanometers and a spherical shape, as shown in TEM. The X-ray diffraction patterns for the nanoparticles, which show face-centered cubic (FCC) of copper, match the crystal structure of Cu@sio2 we discovered using fourier transform infrared (FT-IR) spectroscopy, the fourier transform infrared interaction between the silica and the synthesized copper NPs was investigated. This revealed the capping of the CuNPs by SiO2. The inhibition zone was evident as a result of the activities of these compounds (14, 14, 16, and 20) and (24, 24, 28, and 30) against Escherichia coli bacteria and Staphylococcus aureus bacteria, respectively.