用溶胶-凝胶化学方法研究二氧化硅核壳纳米铜作为抗菌剂

Alaa F. Hashim Al- Ajeeli, Khalid. H. Razeg, Ibrahim Fuad Tariq
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引用次数: 0

摘要

在溶胶凝胶中通过化学反应制备了核壳Cu@sio2纳米粒子,并对其抑制金黄色葡萄球菌和大肠杆菌的能力进行了测试。在合成过程中,利用紫外可见光谱对其进行了表征,在封装前后分别在625纳米和635纳米波长处可见到铜带,这两个波长分别为表面等离子共振频段。利用场发射扫描电镜(FESEM)进一步证实了Cu @Sio2核壳纳米颗粒的生成。TEM显示,核壳纳米粒子的平均尺寸为66纳米,呈球形。纳米粒子的x射线衍射图显示为面心立方(FCC)铜,与我们利用傅里叶变换红外(FT-IR)光谱发现的Cu@sio2晶体结构相匹配,并研究了二氧化硅与合成的铜NPs的傅里叶变换红外相互作用。这揭示了cbp的SiO2盖层。这些化合物(14、14、16和20)和(24、24、28和30)分别对大肠杆菌和金黄色葡萄球菌具有明显的抑制作用。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Copper At Silica Core - Shell Nanoparticles As Antibacterial Agents By Sol-Gel Chemical Methods
Core-shell Cu@sio2 nanoparticles were created by a chemical reaction in a sol gel, and their ability to inhibit S. aureus and E. coli bacteria was tested, when synthesized and characterized using ultraviolet-visible spectroscopy, a copper band could be seen before and after encapsulation at wavelengths of 625 nanometers and 635 nanometers, which are surface plasmonic resonant frequency bands, respectively. The production of Cu @Sio2 core shell nanoparticles was further confirmed using field emission scanning electron microscope (FESEM) pictures. The core shell nanoparticles have a mean size of 66 nanometers and a spherical shape, as shown in TEM. The X-ray diffraction patterns for the nanoparticles, which show face-centered cubic (FCC) of copper, match the crystal structure of Cu@sio2 we discovered using fourier transform infrared (FT-IR) spectroscopy, the fourier transform infrared interaction between the silica and the synthesized copper NPs was investigated. This revealed the capping of the CuNPs by SiO2. The inhibition zone was evident as a result of the activities of these compounds (14, 14, 16, and 20) and (24, 24, 28, and 30) against Escherichia coli bacteria and Staphylococcus aureus bacteria, respectively.
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