激光粉末床熔融增材制造IN738LC的显微组织

Nandana Menon, Tanjheel H. Mahdi, A. Basak
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引用次数: 4

摘要

镍基高温合金在高温下具有优异的蠕变强度和抗疲劳性能,因此广泛用于燃气轮机热截面部件的生产。这种性能的改善是由于在凝固镍的通常面心立方(FCC)结构中存在Ni3Ti或Ni3Al (γ′相)等沉淀强化相。虽然这第二相是性能改善的主要原因,但这种相的存在也增加了加工难度,因为这些合金容易形成裂纹。在这项工作中,在Coherent Creator激光粉末床熔合(L-PBF)增材制造(AM)设备上制备了IN738LC样品。采用光学显微镜(OM)、扫描电镜(SEM)、电子背散射衍射(EBSD)和x射线衍射(XRD)对沉积区进行了表征。在整个沉积区域实现了冶金连续性,并且样品没有显示任何翘曲。然而,样品在沉积区域显示孔洞(如孔隙和裂纹)。结果表明:孔洞面积百分比沿建高方向减小;通过XRD和EBSD证实,沉积的IN738LC在整个沉积区域均呈多晶状。晶粒尺寸也显示出沿构建方向的变化。总之,该结果为学术研究人员和小型企业在台式激光粉末床熔融AM设备上制造高γ′镍基高温合金提供了机会。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Microstructure of IN738LC Fabricated Using Laser Powder Bed Fusion Additive Manufacturing
Nickel-base superalloys are extensively used in the production of gas turbine hot-section components as they offer exceptional creep strength and superior fatigue resistance at high temperatures. Such improved properties are due to the presence of precipitate-strengthening phases such as Ni3Ti or Ni3Al (γ′ phases) in the normally face-centered cubic (FCC) structure of the solidified nickel. Although this second phase is the main reason for the improvements in properties, the presence of such phases also results in increased processing difficulties as these alloys are prone to crack formation. In this work, specimens of IN738LC are fabricated on a Coherent Creator laser powder bed fusion (L-PBF) additive manufacturing (AM) equipment. Optical microscopy (OM), scanning electron microscopy (SEM), electron backscatter diffraction (EBSD), and X-Ray diffraction (XRD) are carried out to characterize the deposit region. Metallurgical continuity is achieved in the entire deposit region and the specimens do not show any warpage. However, the specimens show voids (e.g., pores and cracks) in the deposit region. The results show that the percentage void area decreases along the build height direction. The deposited IN738LC shows polycrystalline grains in the entire deposit region as confirmed by XRD and EBSD. The grain size also shows variations along the build direction. In summary, the results open opportunities for academic researchers and small-scale businesses in fabricating high-γ′ nickel-base superalloys on a desktop laser powder bed fusion AM equipment.
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