溶胶-凝胶法制备316L不锈钢基板HAP涂层

F. Ak Azem, A. Cakir
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引用次数: 3

摘要

近年来,合成羟基磷灰石(HAP)引起了人们的极大兴趣,因为人们寻求能够促进快速骨整合和具有更长的使用寿命的新一代植入物。羟基磷灰石是骨的主要无机成分,已越来越多地用作生物陶瓷涂层,用于承重植入物,以改善对天然骨组织的固定。本研究采用溶胶-凝胶法在316L不锈钢基体上合成HAP涂层,并在不同的煅烧温度下进行热处理。利用x射线衍射光谱(XRD)、傅里叶变换红外光谱(FTIR)和扫描电子显微镜(SEM)对HAP等化合物的形成进行了鉴定和表征。结果表明,涂层的结晶度、结构和形貌随煅烧温度的变化而变化。500℃煅烧后的HAP涂层表面形貌为多孔无裂纹结构。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Production of HAP coating on 316L stainless steel substrates by sol-gel technique
In recent years, synthetic hydroxyapatite (HAP) has attracted much interest because of the quest for new generation implants able to promote rapid osteointegration and having longer lifetimes. HAP a major inorganic component of bone, has been increasingly used as a bioceramic coating for load-bearing implants to improve fixation to natural bone tissue. In this study, HAP coating was synthesized using a sol-gel processing on 316L stainless steel substrate and heat treated at different calcination temperatures. The formation of HAP and other compounds were identified and characterized using X-ray diffraction spectroscopy (XRD), Fourier Transform Infrared (FTIR) and Scanning Electron Microscopy (SEM). It was found that crystallinity, structure and morphology of the coatings varied depending on calcination temperature of the layer. The surface morphology of the HAP coating calcined at 500°C displayed porous and crack free structure.
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