牛和羊骨的成分和热化学分析

O. Ojo, I. Sekunowo, M. Ilomuanya, Philip O. Gbenebor, S. Adeosun
{"title":"牛和羊骨的成分和热化学分析","authors":"O. Ojo, I. Sekunowo, M. Ilomuanya, Philip O. Gbenebor, S. Adeosun","doi":"10.30572/2018/kje/120305","DOIUrl":null,"url":null,"abstract":"Studies have been carried out on bovine bone due to its abundance and large quantity of hydroxyapatite (HAP) in it while caprine bone has been understudied. In this study, locally sourced bovine and caprine bones were washed in distilled water, defatted at 120°C for 1.5 hr in a pressure pot, ball-milled, sieved to 150 µm particle size and characterised. The X-ray fluorescence (XRF) and Energy dispersive X-Ray Spectroscopy (EDS) analysis revealed calcium, phosphorus and carbon as the main components. Both bones contained carbon and oxygen due to the presence of organic collagen but the quantity in caprine bone was a bit higher as revealed by the Fourier Transform Infrared Spectroscopy (FTIR) and EDS spectra. A slight difference in thermal decomposition patterns was recorded while X-Ray diffraction analysis (XRD) revealed the presence of identical functional phases. The microstructures showed needle-like and pebble-like shapes for bovine and caprine respectively, also on visual examination of the Scanning Electron Micrograph (SEM), the bovine samples tended to have particle surface roughness more than caprine. Consequently, the chemical properties of both bone raw samples were insignificantly different from each other except for collagen composition and morphology.","PeriodicalId":123515,"journal":{"name":"Kufa Journal of Engineering","volume":"142 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2021-07-31","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"2","resultStr":"{\"title\":\"COMPOSITIONS AND THERMO-CHEMICAL ANALYSIS OF BOVINE AND CAPRINE BONES\",\"authors\":\"O. Ojo, I. Sekunowo, M. Ilomuanya, Philip O. Gbenebor, S. Adeosun\",\"doi\":\"10.30572/2018/kje/120305\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"Studies have been carried out on bovine bone due to its abundance and large quantity of hydroxyapatite (HAP) in it while caprine bone has been understudied. In this study, locally sourced bovine and caprine bones were washed in distilled water, defatted at 120°C for 1.5 hr in a pressure pot, ball-milled, sieved to 150 µm particle size and characterised. The X-ray fluorescence (XRF) and Energy dispersive X-Ray Spectroscopy (EDS) analysis revealed calcium, phosphorus and carbon as the main components. Both bones contained carbon and oxygen due to the presence of organic collagen but the quantity in caprine bone was a bit higher as revealed by the Fourier Transform Infrared Spectroscopy (FTIR) and EDS spectra. A slight difference in thermal decomposition patterns was recorded while X-Ray diffraction analysis (XRD) revealed the presence of identical functional phases. The microstructures showed needle-like and pebble-like shapes for bovine and caprine respectively, also on visual examination of the Scanning Electron Micrograph (SEM), the bovine samples tended to have particle surface roughness more than caprine. Consequently, the chemical properties of both bone raw samples were insignificantly different from each other except for collagen composition and morphology.\",\"PeriodicalId\":123515,\"journal\":{\"name\":\"Kufa Journal of Engineering\",\"volume\":\"142 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2021-07-31\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"2\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Kufa Journal of Engineering\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.30572/2018/kje/120305\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Kufa Journal of Engineering","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.30572/2018/kje/120305","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 2

摘要

由于牛骨中羟基磷灰石(HAP)的丰富和大量,人们对牛骨进行了研究,而对羊骨的研究还不充分。在这项研究中,当地采购的牛和羊骨在蒸馏水中洗涤,在120°C的压力罐中脱脂1.5小时,球磨,筛选到150µm的粒度并进行表征。x射线荧光(XRF)和能量色散x射线光谱(EDS)分析表明,钙、磷和碳是主要成分。由于有机胶原蛋白的存在,两种骨骼都含有碳和氧,但通过傅里叶变换红外光谱(FTIR)和EDS光谱显示,山羊骨骼中的碳和氧含量略高。热分解模式略有不同,而x射线衍射分析(XRD)显示存在相同的功能相。牛和山羊的显微结构分别表现为针状和卵石状,并且在扫描电镜(SEM)上,牛样品的颗粒表面粗糙度大于山羊样品。因此,除了胶原组成和形态外,两种骨原料样品的化学性质没有显著差异。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
COMPOSITIONS AND THERMO-CHEMICAL ANALYSIS OF BOVINE AND CAPRINE BONES
Studies have been carried out on bovine bone due to its abundance and large quantity of hydroxyapatite (HAP) in it while caprine bone has been understudied. In this study, locally sourced bovine and caprine bones were washed in distilled water, defatted at 120°C for 1.5 hr in a pressure pot, ball-milled, sieved to 150 µm particle size and characterised. The X-ray fluorescence (XRF) and Energy dispersive X-Ray Spectroscopy (EDS) analysis revealed calcium, phosphorus and carbon as the main components. Both bones contained carbon and oxygen due to the presence of organic collagen but the quantity in caprine bone was a bit higher as revealed by the Fourier Transform Infrared Spectroscopy (FTIR) and EDS spectra. A slight difference in thermal decomposition patterns was recorded while X-Ray diffraction analysis (XRD) revealed the presence of identical functional phases. The microstructures showed needle-like and pebble-like shapes for bovine and caprine respectively, also on visual examination of the Scanning Electron Micrograph (SEM), the bovine samples tended to have particle surface roughness more than caprine. Consequently, the chemical properties of both bone raw samples were insignificantly different from each other except for collagen composition and morphology.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:481959085
Book学术官方微信