溶液还原法制备纳米Ag2O和Cu(OH)2及其抑菌性能

R. Rajakumari, C. Priya, A. Srilekha
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引用次数: 3

摘要

以硝酸银(agno3)和五水硫酸铜(cuso4.5 h2o)为还原剂,以氢氧化钠(NaOH)为还原剂,采用简单溶液还原法制备了氧化银(ag2o)和氢氧化铜(Cu(OH) 2纳米粒子。通过x射线衍射(XRD)分析、扫描电镜(SEM)分析、傅里叶变换红外光谱(FT-IR)分析、紫外吸收和光致发光(PL)、振动样品磁强计(VSM)研究,确定了合成样品的尺寸分布测量、表面形貌、光学和磁性能。通过x射线衍射(XRD)研究,证实了银纳米粒子以ag2o的形式合成,铜以Cu(OH) 2的形式合成。紫外可见吸收分析表明,Ag 2o的吸收峰位于光谱的较低波长区域。Ag 2o和Cu(OH) 2在FTIR光谱中的尖锐强度峰表明了样品中分子官能团的拉伸和弯曲频率以及它们的高结晶性。SEM图像显示,纳米二氧化银的形状接近球形。Cu(OH) 2的VSM研究在室温下显示出铁磁相互作用。Ag 2o和Cu(OH) 2对金黄色葡萄球菌和大肠杆菌的抑菌性能表明,两种样品对金黄色葡萄球菌均有抑菌效果,且呈浓度依赖性。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and Characterization of Nano Ag2O and Cu(OH)2 by Solution Reduction Method and Their Antibacterial Studies
Silver oxide (Ag 2 O) and copper(II)hydroxide (Cu(OH) 2 ) nanoparticles were synthesized through a simple solution reduction method using silver nitrate (AgNO 3 ) and copper sulphate pentahydrate (CuSO 4 .5H 2 O) in the presence of sodium hydroxide (NaOH) as reducing agent. X-ray diffraction (XRD) analysis, scanning electron microscopic (SEM) analysis, Fourier transform infrared spectroscopic (FT-IR) analysis, UV-absorption and photoluminescence (PL), vibrating sample magnetometer (VSM) studies were performed to confirm the size distribution measurement, surface morphology, optical and magnetic properties of the synthesized samples. Silver nanoparticles synthesized in the form of Ag 2 O and copper in the form of Cu(OH) 2 was confirmed by the XRD study. The UV-Vis absorption analysis indicates that the absorption peak for Ag 2 O in the lower wavelength region of the optical spectrum. The sharp intensity peaks in the FTIR spectrum of Ag 2 O and Cu(OH) 2 indicate the stretching and bending frequencies of the molecular functional groups in the samples as well as their high crystalline nature. The SEM images show the shape of Ag 2 O nanoparticles is nearly spheroid. The VSM study of Cu(OH) 2 shows ferromagnetic interaction at room temperature. The antibacterial properties of Ag 2 O and Cu(OH) 2 on Staphylococcus aureus and Escherichia coli indicate that both the samples are effective on Staphylococcus aureus , which is concentration dependent.
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