具有(HL)4 PE-Si3N4/PE-SiO2反射器的VIS fabry - p干涉仪在独立LP-Si3N4膜上用于表面增强拉曼光谱

SPIE OPTO Pub Date : 2016-03-15 DOI:10.1117/12.2208567
C. Helke, M. Meinig, M. Seifert, J. Seiler, K. Hiller, S. Kurth, Jörg Martin, T. Gessner
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引用次数: 7

摘要

小型化光谱系统的深入发展使新的突破性应用成为可能,例如通过表面增强拉曼光谱(SERS)对特定分子进行在线监测系统。该光谱系统基于原位生成纳米粒子的SERS活性表面和小型化探测器,配备可调谐的fabry - p干涉仪(FPI),具有非常尖锐的透射峰和低于2 nm的FWHM带宽。该在线监测系统的关键部分是采用MEMS技术制作的可调谐FPI。这一贡献提出了一个7.5 x 7.5 mm²芯片尺寸的FPI,由210 nm薄且直径高达5.5 mm的硅载体上的可移动反射器和玻璃上的固定反射器组成。在570 nm的中心波长处设计了孔径为2mm的光学谐振腔,利用硅在玻璃衬底上的SU-8粘接实现。采用湿法和干法相结合的方法制备了可移动氮化硅膜。采用PE-CVD方法在LP-CVD-Si3N4上沉积了反射率为93%的介质(HL)4 Si3N4/ SiO2反射器叠层,并在膜和玻璃上进行了干蚀刻。测得的峰值透过率在52% ~ 74%之间,频宽在1.3 ~ 2.0 nm之间。结果表明,fpi可以在555 nm至585 nm的光谱范围内调谐,这与该SERS应用相关,调谐电压为25 V。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
VIS Fabry-Pérot-Interferometer with (HL)4 PE-Si3N4/PE-SiO2 reflectors on freestanding LP-Si3N4 membranes for surface enhanced Raman spectroscopy
Profound developments of miniaturized spectrometry systems enable new breakthrough applications such as online monitoring systems for specific molecules by Surface Enhanced Raman Spectroscopy (SERS). The spectrometry system is based on SERS active surfaces in-situ generating nanoparticles and miniaturized detectors with tunable Fabry-Pérot- Interferometers (FPI) with very sharp transmission peaks and a FWHM bandwidth below 2 nm. The key part of this online monitoring system is a tunable FPI, which is fabricated with MEMS technology. This contribution presents a 7.5 x 7.5 mm² chip size FPI, consisting of a moveable reflector on a 210 nm thin and up to 5.5 mm in diameter Si3N4 membrane on a silicon carrier, and a fixed reflector on glass. The optical resonator with an aperture of 2 mm diameter is designed for the central wavelength of 570 nm and realized by adhesive SU-8 bonding of the silicon on glass substrate. The moveable Si3N4 membrane is fabricated by combined wet and dry etching of silicon. The dielectric (HL)4 Si3N4/ SiO2 reflector stack with a reflectance of 93 % is deposited by PE-CVD on the LP-CVD-Si3N4 and structured by dry etching on the membrane and the glass. The measured peak transmittance is between 52 % and 74 % with a FWHM bandwidth between 1.3 nm and 2.0 nm. It was shown, that the FPIs are tunable over the spectral range from 555 nm to 585 nm which is relevant for this SERS application with a tuning voltage of 25 V.
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