使用视频点播教育目的:从三个月的实验观察

Pierre C. Bélanger, S. Clément
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引用次数: 1

摘要

由烟酸- n -氧化物生产2-氯烟酸的工艺,其特点是将2-氯烟酸氯从反应混合物中蒸馏出来,并使馏出物在40℃至100℃的温度下流入水中,2-氯烟酸氯水解成2-氯烟酸,该2-氯烟酸氯以纯白色结晶形式沉淀。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Using Video-On-Demand For Educational Purposes: Observations from a Three Month Experiment
The process for the production of 2-chloronicotinic acid from nicotinic acid-N-oxide, characterized in that the 2-chloronicotinic acid chloride is distilled off from the reaction mixture and the distillate is allowed to flow into water at a temperature of 40 DEG to 100 DEG C. The 2-chloronicotinic acid chloride is hydrolized to the 2-chloronicotinic acid, which precipitates in a pure white crystalline form.
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