{"title":"等离子体氮化及其对不锈钢1.4006耐蚀性的影响","authors":"M. Krbaťa, Robert Ciger","doi":"10.21496/ams.2021.022","DOIUrl":null,"url":null,"abstract":": The plasma nitriding (PN) technology was applied on the martensitic stainless steel 1.4006. The influence of PN on the corrosion resistance of selected material was investigated. The chemical composition of selected steel was verified using the Q4 TASMAN device. The PN process was performed using two stage nitriding procedure. After plasma cleaning procedure at 515 °C for 45 min in a nitriding atmosphere ratio 20H2:2N2 (l/h) was the first stage nitriding procedure performed at 520°C for 16 hours in a nitriding atmosphere ratio 25H2:5N2 (l/h) and followed by the second stage of nitriding procedure performed at 525°C for 4 hours in a nitriding atmosphere ratio 28H2:4N2 (l/h). The microstructure and mechanical properties of the nitride layers were studied using OES spectrometry, optical microscopy, and hardness testing. The depths of plasma nitride layers were also estimated using a cross-sectional microhardness profiles measurement. The corrosion resistance testing of PN stainless steel 1.4006 samples were carried out in a 5 % neutral sodium chloride solution (NSS) in accordance with ISO 9227 standard in the VLM GmbH SAL 400-FL corrosion chamber and visually evaluated. Microhardness and surface hardness of experimental samples were significantly increased, but the corrosion resistance remarkably decreased.","PeriodicalId":135905,"journal":{"name":"Acta Mechanica Slovaca","volume":"82 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2022-06-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Plasma Nitriding and Its Effect on the Corrosion Resistance of Stainless Steel 1.4006\",\"authors\":\"M. Krbaťa, Robert Ciger\",\"doi\":\"10.21496/ams.2021.022\",\"DOIUrl\":null,\"url\":null,\"abstract\":\": The plasma nitriding (PN) technology was applied on the martensitic stainless steel 1.4006. The influence of PN on the corrosion resistance of selected material was investigated. The chemical composition of selected steel was verified using the Q4 TASMAN device. The PN process was performed using two stage nitriding procedure. After plasma cleaning procedure at 515 °C for 45 min in a nitriding atmosphere ratio 20H2:2N2 (l/h) was the first stage nitriding procedure performed at 520°C for 16 hours in a nitriding atmosphere ratio 25H2:5N2 (l/h) and followed by the second stage of nitriding procedure performed at 525°C for 4 hours in a nitriding atmosphere ratio 28H2:4N2 (l/h). The microstructure and mechanical properties of the nitride layers were studied using OES spectrometry, optical microscopy, and hardness testing. The depths of plasma nitride layers were also estimated using a cross-sectional microhardness profiles measurement. The corrosion resistance testing of PN stainless steel 1.4006 samples were carried out in a 5 % neutral sodium chloride solution (NSS) in accordance with ISO 9227 standard in the VLM GmbH SAL 400-FL corrosion chamber and visually evaluated. Microhardness and surface hardness of experimental samples were significantly increased, but the corrosion resistance remarkably decreased.\",\"PeriodicalId\":135905,\"journal\":{\"name\":\"Acta Mechanica Slovaca\",\"volume\":\"82 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-06-01\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Acta Mechanica Slovaca\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.21496/ams.2021.022\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Acta Mechanica Slovaca","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.21496/ams.2021.022","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
对马氏体不锈钢1.4006进行了等离子体氮化处理。研究了PN对所选材料耐腐蚀性能的影响。采用Q4 TASMAN装置对所选钢的化学成分进行了验证。PN工艺采用两级渗氮工艺。在515°C、20H2:2N2 (l/h)的渗氮气氛下,在515°C、45分钟的等离子清洗过程后,在520°C、25H2:5N2 (l/h)的渗氮气氛下,进行第一步渗氮过程,持续16小时,然后在525°C、28H2:4N2 (l/h)的渗氮气氛下,进行第二阶段渗氮过程,持续4小时。采用OES光谱法、光学显微镜和硬度测试研究了氮化层的显微组织和力学性能。等离子体氮化层的深度也可以用横截面显微硬度测量来估计。在VLM GmbH SAL 400-FL腐蚀室中,按照ISO 9227标准,在5%中性氯化钠溶液(NSS)中进行了PN不锈钢1.4006样品的耐蚀性测试,并进行了目测评价。实验样品的显微硬度和表面硬度显著提高,但耐蚀性显著降低。
Plasma Nitriding and Its Effect on the Corrosion Resistance of Stainless Steel 1.4006
: The plasma nitriding (PN) technology was applied on the martensitic stainless steel 1.4006. The influence of PN on the corrosion resistance of selected material was investigated. The chemical composition of selected steel was verified using the Q4 TASMAN device. The PN process was performed using two stage nitriding procedure. After plasma cleaning procedure at 515 °C for 45 min in a nitriding atmosphere ratio 20H2:2N2 (l/h) was the first stage nitriding procedure performed at 520°C for 16 hours in a nitriding atmosphere ratio 25H2:5N2 (l/h) and followed by the second stage of nitriding procedure performed at 525°C for 4 hours in a nitriding atmosphere ratio 28H2:4N2 (l/h). The microstructure and mechanical properties of the nitride layers were studied using OES spectrometry, optical microscopy, and hardness testing. The depths of plasma nitride layers were also estimated using a cross-sectional microhardness profiles measurement. The corrosion resistance testing of PN stainless steel 1.4006 samples were carried out in a 5 % neutral sodium chloride solution (NSS) in accordance with ISO 9227 standard in the VLM GmbH SAL 400-FL corrosion chamber and visually evaluated. Microhardness and surface hardness of experimental samples were significantly increased, but the corrosion resistance remarkably decreased.