用共沉淀法合成不同苯胺二聚体- cooh的磁铁矿(Fe3O4)纳米颗粒及表征

Z. I. Takai, M. K. Mustafa, S. Asman
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引用次数: 1

摘要

采用辅助共沉淀法制备了含有一定量苯胺二聚体- cooh的磁铁矿(Fe3O4)纳米颗粒的形貌。用场发射扫描电镜(FESEM)观察了Fe3O4纳米颗粒的形貌,结果表明,苯胺二聚体- cooh制备的Fe3O4纳米颗粒团聚,形状和尺寸更接近球形。通过x射线衍射(XRD)对Fe3O4纳米颗粒进行物相分析,结果表明,添加少量苯胺二聚体- cooh制备的Fe3O4纳米颗粒比未添加苯胺二聚体制备的Fe3O4纳米颗粒具有更多的峰。然而,利用傅里叶变换红外光谱(FTIR)研究了Fe3O4纳米颗粒的分子结构和官能团,结果证明了分子存在Fe-O波段。采用辅助共沉淀法制备了含有一定量苯胺二聚体- cooh的磁铁矿(Fe3O4)纳米颗粒的形貌。用场发射扫描电镜(FESEM)观察了Fe3O4纳米颗粒的形貌,结果表明,苯胺二聚体- cooh制备的Fe3O4纳米颗粒团聚,形状和尺寸更接近球形。通过x射线衍射(XRD)对Fe3O4纳米颗粒进行物相分析,结果表明,添加少量苯胺二聚体- cooh制备的Fe3O4纳米颗粒比未添加苯胺二聚体制备的Fe3O4纳米颗粒具有更多的峰。然而,利用傅里叶变换红外光谱(FTIR)研究了Fe3O4纳米颗粒的分子结构和官能团,结果证明了分子存在Fe-O波段。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and characterization of magnetite (Fe3O4) nanoparticles with different level of aniline dimer-COOH by co precipitation method
The morphologies of the magnetite (Fe3O4) nanoparticles with certain level of aniline dimer-COOH were prepared via assisted co-precipitation method. The Fe3O4 nanoparticles morphologies are observed by Field Emission Scanning Electron Microscope (FESEM) and the result shows that, the Fe3O4 nanoparticles prepared with aniline dimer-COOH is agglomerated and more spherical in shape and size. The phase analysis of the Fe3O4 nanoparticles was perform by X-ray Diffraction spectra (XRD), the result indicates that, the particles prepared with littlie amount of aniline dimer-COOH have more peaks compare to the uncapped Fe3O4 nanoparticles. However, the molecular structure and functional group of Fe3O4 nanoparticles were studied using Fourier Transform Infrared Spectra (FTIR) and the result proven the appearance Fe-O band of the molecules.The morphologies of the magnetite (Fe3O4) nanoparticles with certain level of aniline dimer-COOH were prepared via assisted co-precipitation method. The Fe3O4 nanoparticles morphologies are observed by Field Emission Scanning Electron Microscope (FESEM) and the result shows that, the Fe3O4 nanoparticles prepared with aniline dimer-COOH is agglomerated and more spherical in shape and size. The phase analysis of the Fe3O4 nanoparticles was perform by X-ray Diffraction spectra (XRD), the result indicates that, the particles prepared with littlie amount of aniline dimer-COOH have more peaks compare to the uncapped Fe3O4 nanoparticles. However, the molecular structure and functional group of Fe3O4 nanoparticles were studied using Fourier Transform Infrared Spectra (FTIR) and the result proven the appearance Fe-O band of the molecules.
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