含Co和Ni纳米粒子的聚乙烯杂化磁性材料

A. Vasil'kov, A. Budnikov, A. Naumkin
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引用次数: 1

摘要

采用金属气相合成法制备了以HDPE为基材,填充Со和Ni纳米粒子的新型杂化磁性材料。阐明了金属-聚合物复合材料的性能是MVS参数和金属性质的函数。法拉第方法已被用于表征系统的磁性。利用XRD、EXAFS和SAXS等x射线和同步加速器技术对样品的微观结构进行了研究。用XPS测定了核能级和价带光谱。在c1s谱中,C- ni键的结合能峰值为282.8 eV。结果表明,相似组成的纳米复合材料的性能是由合成条件和合成后因素共同决定的。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Hybrid magnetic materials based on polyethylene containing Co and Ni nanoparticles
New hybrid magnetic materials based on HDPE filled with Со and Ni nanoparticles have been prepared via the metal vapor synthesis. Properties of the metal-polymer composites have been elucidated as a function of MVS parameters and metal nature. The Faraday method has been applied to characterize the magnetic properties of the systems. The microstructure of the samples has been studied with a number of X-ray and synchrotron techniques, including XRD, EXAFS and SAXS. Core-level and valence band spectra were measured by XPS. The peak at binding energy of 282.8 eV characteristic of C-Ni bond was recorded in the C 1s spectrum. It was shown that properties of nanocomposite materials with similar compositions are determined both by the synthesis conditions and post-synthesis factors.
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