工业纯钛搅拌摩擦加工的力学性能及腐蚀行为分析

Senthil Kumar Velukkudi Santhanam, Joshua Richard Jeyarajan, S. Manivannan, Joseph Beski Jayamanickam, Raman Kuppusamy, Nitin Nambi
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引用次数: 0

摘要

搅拌摩擦加工是一种理想的细化晶粒的方法,提高了材料的成形性、显微硬度、屈服强度和抗拉强度等力学性能,提高了材料的耐腐蚀性,是一种选择性表面改性的有效方法,同时也保持了材料的整体性能。在本研究中,我们选择了2级钛(商业纯钛)作为材料,因为它比其他等级的钛具有更好的耐腐蚀性,高抗拉强度和高硬度。由于其柔软、优异的耐腐蚀性能和延展性,Cp - Ti被用于汽车零部件和机身结构。搅拌摩擦处理被用来改善机械性能,如拉伸和显微硬度,以及腐蚀性能。摩擦搅拌加工(FSP)是用来制造钛板,通过改变工艺参数,如刀具转速(rpm),横移速度(mm/min),和通道数。本实验采用的工艺参数为:刀具转速为1000rpm、1200rpm、1400rpm,横移速度为30mm /min、45mm /min、60mm /min,单道、双道、三道。实验采用田口L9正交阵列,在三个不同的水平上考虑三个参数。设计和制造了洛氏硬度为65 HRC的HSS(高速钢)锥形圆柱销,以提供材料流动,同时最大限度地减少刀具磨损。拉伸试验采用ASTM E8标准通用试验机(UTM)确定FSPed CP - Ti(2级)的极限拉伸强度和屈服强度,显微硬度试验采用金刚石压头维氏硬度,腐蚀值采用浸入式腐蚀试验方法,根据ASTM G31 - 72标准称重样品的前后重量。由于2级钛具有非常高的耐腐蚀性,因此在24小时内完成的腐蚀速率可以忽略不计。因此,浸泡腐蚀试验进行超过120小时,因此可以有效地测量腐蚀速率。同时计算这个过程中产生的力矩。通过将测试结果作为输入,对拉伸强度、显微硬度和耐腐蚀性等多个测试结果进行灰色关联分析(GRA),以找到最佳工艺参数。方差分析(ANOVA)是分析搅拌摩擦处理实验数据最有效的参数化方法。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Analysis on Mechanical Properties and Corrosion Behavior of Friction Stir Processing of Commercially Pure-Titanium
Friction Stir Processing has become the ideal way to refine the grains which increases the mechanical properties like formability, microhardness, yield strength and Tensile Strength, also increases the corrosion resistance, which emerged as the effective way for selective surface modification and also retaining the bulk properties. In this present work, Titanium grade 2 (Commercially Pure Titanium) is selected as the material of choice due to its superior corrosion resistance compared to other grades of titanium, high tensile strength and high hardness. Due to soft, excellent corrosion resistance and ductile properties Cp - Ti is used in automotive parts and airframe structure application. Friction stir processing is being used to improve mechanical properties such as tensile and microhardness, as well as corrosion properties. Friction stir processing (FSP) is used to fabricate the Titanium plate, by varying the process parameters such as Tool Rotation Speed (rpm), Traverse Speed (mm/min), and Number of Passes. The process parameters used in this experiment are Tool Rotational speed of 1000 rpm, 1200 rpm and 1400 rpm, Traverse speed of 30 mm/min, 45 mm/min, and 60 mm/min and single pass, double pass and triple pass. Taguchi’s L9 Orthogonal array is used to conduct the experiment, which considers three parameters at three separate levels. A tapered cylindrical pin of HSS (High Speed Steel) with Rockwell hardness of 65 HRC is designed and fabricated to provide material flow while simultaneously minimizing the tool wear. The tensile test was carried out using Universal Testing Machine (UTM) as per ASTM E8 standard to determine the ultimate tensile strength and yield strength of FSPed CP – Ti (grade 2), microhardness test was carried out using Vickers Hardness with a diamond indenter and corrosion values are evaluated using Immersion corrosion testing method by weighing the before and after weights of the sample as per ASTM G31 – 72. Since Titanium Grade 2 offers very high corrosion resistance, the rate of corrosion is negligible when done in 24 hours. Thus, immersion corrosion test is done over 120 hours, so that corrosion rate can be measured efficiently. And also evaluate the torque induced in this process. Grey Relational Analysis (GRA) is performed on the multiple test results such that tensile strength, microhardness and corrosion resistances to find the optimum process parameters, by applying the test results as inputs. Analysis of variance (ANOVA) is the most efficient parametric method for analyzing friction stir processing data from experiments results.
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