成核法和生长法化学合成纳米银的光学和形态分析比较

S. Lavanya, G. Paramasivam, G. Maragathavalli
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引用次数: 0

摘要

本研究的目的是利用成核和生长方法对化学合成的纳米银颗粒进行光学和形态学分析,并与尺寸和吸光度进行比较。以硝酸银为原料,以硼氢化钠(N aBH4)为盖层剂,柠檬酸钠为盖层剂,合成了化学合成的纳米银。这里分析了7组,总样本量为26。采用紫外可见光谱(UV- vis)和扫描电镜(SEM)对纳米颗粒进行了表征。对样品的吸光度和形貌进行了分析。纳米粒子在不同波长具有不同的吸光度。对纳米粒子的吸光度进行分析是十分必要的。从200-700 nm对颗粒进行分析。它在可见光区有很高的吸光度,约400-420 nm,在紫色区。利用扫描电镜对其形貌进行分析,确定其尺寸分布。它的平均尺寸为9.5纳米。采用形貌(SEM)分析了颗粒的尺寸分布。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Comparison of Optical and Morphological Analysis of Chemically Synthesized Silver Nanoparticles using Nucleation and Growth method
The aim of this study is to do the optical and morphological analysis of chemically synthesized silver nanopar-ticles using nucleation and growth methods as compared with size and absorbance. Chemically synthesized silver nanoparticles were synthesized by silver nitrate with sodium borohydride (N aBH4) in the presence of sodium citrate as capping agent. Here seven groups were analyzed and the total sample size was 26. The nanoparticle was characterized by the means of UV Visible (UV-Vis) spectroscopy and scanning and electron microscopy (SEM).The absorbance and morphology is analysed of the samples. Nanoparticles are having different absorbances in different wavelengths. It is very essential to analyse the absorbance of the nanoparticles. The particle was analysed from 200–700 nm. It has high absorbance in the visible region about 400–420 nm which is in the violet region. The morphology is analysed using SEM to determine the size distribution. It has an average size of 9.5 nm. The morphology (SEM) is taken to analyse the size distribution of the particle.
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