猪骨的热刺激电流分析

Zhu Yafei, W. Zonghan, Xu Fudong
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引用次数: 0

摘要

粗骨的TSC(热刺激电流)谱在75℃时出现10/sup -8/ A的峰值。在第一个周期后立即进行的TSC实验的第二个周期中,该峰消失。样品暴露在大气中几天后,它又出现了。当样品翻转时,峰的方向没有改变。样品完全干燥后,75℃时峰消失。另一个峰出现在95℃左右,比75℃时的峰小得多,而且它的方向不能通过翻转样品来逆转。x射线衍射和红外吸收作为互补分析技术。从这些实验中可以看出,较大的峰来自自由水,较小的峰来自结晶水、角蛋白和肽等。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
The analysis of thermally stimulated current of pig bone
A peak of 10/sup -8/ A was found at 75 degrees C in the TSC (thermally stimulated current) spectrum of crude bone. This peak disappeared in the second cycle of a TSC experiment performed immediately after the first cycle. It reappeared after the sample was exposed to the atmosphere for a few days. When the sample was turned over, the direction of the peak was not changed. After the sample was dried completely, the peak at 75 degrees C disappeared. Another peak, which was much smaller than the peak at 75 degrees C, appeared around 95 degrees C, and its direction could not be reversed by turning the sample over. X-ray diffraction and infrared absorption were used as complementary analysis techniques. It is concluded from these experiments that the larger peak originated from the free water and the smaller one is due to crystallization water, keratin and peptide, etc.<>
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