{"title":"自蔓延高温合成法生产腐蚀合金","authors":"M. Kozhanova, M. Boronenko, V. Zelensky","doi":"10.18822/byusu20220222-29","DOIUrl":null,"url":null,"abstract":"The subject of research: Self-propagating high-temperature synthesis (SHS) is an energetically low-cost method for obtaining materials with desired properties. \nThe purpose of research: Development and approbation of the method of self-propagating high-temperature synthesis. \nMethods and objects of research: For the synthesis of a corrosion-resistant material, a thermite mixture of Al (75 %) and Fe2O3 (25 %) and the addition of MoO3 with a variable mass fraction of 10 %, 15 %, 20 %, 25 % of thermite were taken. The composition and structure of the synthesized material were determined by XRD and metallography methods. Based on the properties of the physical properties of the obtained material (porosity, electrical conductivity) and its phase composition (MoO2, Al2O3, FeMoO4), samples obtained with a 15 % addition of MoO3 were selected for testing for corrosion resistance. \nResults of research: The paper presents the results of approbation of obtaining a corrosion-resistant material by the SHS method. Conducted tests for corrosion resistance established: the rate of continuous corrosion of the synthesized material (MoO3 15 %) was 0.2 mm / year, which is close in value to corrosion-resistant steels; high resistance of the synthesized material to technical salt when tested for 14 days with a concentrated solution of the reagent 0.18 ml * eq / l. The listed properties of the synthesized material confirm the possibility of obtaining corrosion-resistant materials by the SHS method, including those for operation in the Arctic.","PeriodicalId":375097,"journal":{"name":"Yugra State University Bulletin","volume":"100 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2022-08-07","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"The production of corrosion alloy by self-propagating high-temperature synthesis\",\"authors\":\"M. Kozhanova, M. Boronenko, V. Zelensky\",\"doi\":\"10.18822/byusu20220222-29\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"The subject of research: Self-propagating high-temperature synthesis (SHS) is an energetically low-cost method for obtaining materials with desired properties. \\nThe purpose of research: Development and approbation of the method of self-propagating high-temperature synthesis. \\nMethods and objects of research: For the synthesis of a corrosion-resistant material, a thermite mixture of Al (75 %) and Fe2O3 (25 %) and the addition of MoO3 with a variable mass fraction of 10 %, 15 %, 20 %, 25 % of thermite were taken. The composition and structure of the synthesized material were determined by XRD and metallography methods. Based on the properties of the physical properties of the obtained material (porosity, electrical conductivity) and its phase composition (MoO2, Al2O3, FeMoO4), samples obtained with a 15 % addition of MoO3 were selected for testing for corrosion resistance. \\nResults of research: The paper presents the results of approbation of obtaining a corrosion-resistant material by the SHS method. Conducted tests for corrosion resistance established: the rate of continuous corrosion of the synthesized material (MoO3 15 %) was 0.2 mm / year, which is close in value to corrosion-resistant steels; high resistance of the synthesized material to technical salt when tested for 14 days with a concentrated solution of the reagent 0.18 ml * eq / l. The listed properties of the synthesized material confirm the possibility of obtaining corrosion-resistant materials by the SHS method, including those for operation in the Arctic.\",\"PeriodicalId\":375097,\"journal\":{\"name\":\"Yugra State University Bulletin\",\"volume\":\"100 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2022-08-07\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"Yugra State University Bulletin\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.18822/byusu20220222-29\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"Yugra State University Bulletin","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.18822/byusu20220222-29","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
摘要
研究主题:自传播高温合成(SHS)是一种能量低的方法,以获得所需的性能材料。研究目的:发展和认可自传播高温合成方法。研究方法和研究对象:采用Al(75%)和Fe2O3(25%)的铝热剂混合,添加铝热剂质量分数分别为10%、15%、20%、25%的MoO3,合成了一种耐腐蚀材料。采用XRD和金相法对合成材料的组成和结构进行了表征。根据所得材料的物理性质(孔隙率、电导率)及其相组成(MoO2、Al2O3、FeMoO4),选择添加15% MoO3的样品进行耐蚀性测试。研究结果:本文介绍了用SHS法获得耐腐蚀材料的认可结果。进行了耐腐蚀性测试:合成材料的连续腐蚀速率(MoO3 15%)为0.2 mm /年,与耐腐蚀钢的值接近;在试剂0.18 ml * eq / l的浓缩溶液中测试14天后,合成材料对技术盐具有很高的耐腐蚀性。合成材料的列出的性能证实了通过SHS方法获得耐腐蚀材料的可能性,包括在北极操作的材料。
The production of corrosion alloy by self-propagating high-temperature synthesis
The subject of research: Self-propagating high-temperature synthesis (SHS) is an energetically low-cost method for obtaining materials with desired properties.
The purpose of research: Development and approbation of the method of self-propagating high-temperature synthesis.
Methods and objects of research: For the synthesis of a corrosion-resistant material, a thermite mixture of Al (75 %) and Fe2O3 (25 %) and the addition of MoO3 with a variable mass fraction of 10 %, 15 %, 20 %, 25 % of thermite were taken. The composition and structure of the synthesized material were determined by XRD and metallography methods. Based on the properties of the physical properties of the obtained material (porosity, electrical conductivity) and its phase composition (MoO2, Al2O3, FeMoO4), samples obtained with a 15 % addition of MoO3 were selected for testing for corrosion resistance.
Results of research: The paper presents the results of approbation of obtaining a corrosion-resistant material by the SHS method. Conducted tests for corrosion resistance established: the rate of continuous corrosion of the synthesized material (MoO3 15 %) was 0.2 mm / year, which is close in value to corrosion-resistant steels; high resistance of the synthesized material to technical salt when tested for 14 days with a concentrated solution of the reagent 0.18 ml * eq / l. The listed properties of the synthesized material confirm the possibility of obtaining corrosion-resistant materials by the SHS method, including those for operation in the Arctic.