Inconel 718高温合金微等离子体增材制造工艺的发展与表征

J. Nagy, Adrian Singh, Xiao Huang
{"title":"Inconel 718高温合金微等离子体增材制造工艺的发展与表征","authors":"J. Nagy, Adrian Singh, Xiao Huang","doi":"10.31399/asm.cp.itsc2023p0450","DOIUrl":null,"url":null,"abstract":"\n A micro-plasma system was investigated for its capability in additive manufacturing (AM). Micro-plasma AM system has the advantage of lower cost and higher deposition rate over the laser-based AM systems, and generates leaner and cleaner weld deposit than other arc-based AM systems. However, the microplasma system is complex and involves a large number of process variables. In this study, the effects of two arc and wire feed modes on dimensional consistency and hardness were firstly examined. Subsequently, one set of the specimens was further subjected to oxidation tests and the results were compared to that from conventional wrought Inconel 718. It was found that all four processes could produce crack free samples without measurable distortion. Some surface discoloration was observed, ranging from light straw to a purple tint. After heat treatment, the hardness of the samples varies from 403 to 440 HV, with the transverse surface showing slightly lower hardness values. The oxidation tests at 900 °C yielded similar weight change for AM Inconel 718 and its counterpart wrought alloy; however, the rate constant for wrought alloy was slightly higher. Microstructural analysis with SEM and EDS revealed a dendritic structure in the AM Inconel 718 and the presence of Nb-rich compounds in the interdendritic region. The polycrystal grain structure was not delineated in AM material as that in wrought 718. With the increase of exposure time, the oxide layer continues to increase at a higher rate, along with a sublayer of Ni3Nb above the metal substrate. In addition, after 200 hours, the wrought alloy developed porous chromia, while AM material exhibited uneven oxide thickness. In consideration of all aspects of the evaluation carried out thus far, it is concluded that the AM material produced by micro-plasma process is equivalent to wrought material in mechanical properties and oxidation performance.","PeriodicalId":114755,"journal":{"name":"International Thermal Spray Conference","volume":"8 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2023-05-22","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Development and Characterization of Micro-Plasma Additive Manufacturing Process for Inconel 718 Superalloy\",\"authors\":\"J. Nagy, Adrian Singh, Xiao Huang\",\"doi\":\"10.31399/asm.cp.itsc2023p0450\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"\\n A micro-plasma system was investigated for its capability in additive manufacturing (AM). Micro-plasma AM system has the advantage of lower cost and higher deposition rate over the laser-based AM systems, and generates leaner and cleaner weld deposit than other arc-based AM systems. However, the microplasma system is complex and involves a large number of process variables. In this study, the effects of two arc and wire feed modes on dimensional consistency and hardness were firstly examined. Subsequently, one set of the specimens was further subjected to oxidation tests and the results were compared to that from conventional wrought Inconel 718. It was found that all four processes could produce crack free samples without measurable distortion. Some surface discoloration was observed, ranging from light straw to a purple tint. After heat treatment, the hardness of the samples varies from 403 to 440 HV, with the transverse surface showing slightly lower hardness values. The oxidation tests at 900 °C yielded similar weight change for AM Inconel 718 and its counterpart wrought alloy; however, the rate constant for wrought alloy was slightly higher. Microstructural analysis with SEM and EDS revealed a dendritic structure in the AM Inconel 718 and the presence of Nb-rich compounds in the interdendritic region. The polycrystal grain structure was not delineated in AM material as that in wrought 718. With the increase of exposure time, the oxide layer continues to increase at a higher rate, along with a sublayer of Ni3Nb above the metal substrate. In addition, after 200 hours, the wrought alloy developed porous chromia, while AM material exhibited uneven oxide thickness. In consideration of all aspects of the evaluation carried out thus far, it is concluded that the AM material produced by micro-plasma process is equivalent to wrought material in mechanical properties and oxidation performance.\",\"PeriodicalId\":114755,\"journal\":{\"name\":\"International Thermal Spray Conference\",\"volume\":\"8 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2023-05-22\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"International Thermal Spray Conference\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.31399/asm.cp.itsc2023p0450\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"International Thermal Spray Conference","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.31399/asm.cp.itsc2023p0450","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0

摘要

研究了微等离子体系统在增材制造中的性能。与激光增材系统相比,微等离子体增材系统具有成本更低、沉积速率更高的优点,并且与其他电弧增材系统相比,其焊缝沉积物更干净、更清洁。然而,微等离子体系统是复杂的,涉及大量的过程变量。在本研究中,首先考察了两种电弧和送丝方式对尺寸一致性和硬度的影响。随后,对其中一组试样进行了进一步的氧化试验,并将结果与常规锻造Inconel 718的结果进行了比较。结果表明,这四种工艺均能得到无裂纹的试样,且无明显的变形。观察到一些表面变色,从浅稻草色到紫色。热处理后试样的硬度在403 ~ 440 HV之间,横向硬度值略低。在900℃的氧化试验中,增材制造Inconel 718及其对应的变形合金的重量变化相似;而变形合金的速率常数略高。扫描电镜和能谱分析表明,AM Inconel 718中存在枝晶结构,枝晶间存在富铌化合物。增材制造材料的多晶晶粒结构与变形718材料不同。随着暴露时间的增加,氧化层继续以更高的速率增加,并在金属衬底上形成Ni3Nb亚层。此外,在200小时后,变形合金出现多孔铬,而AM材料表现出不均匀的氧化厚度。综合目前所进行的各方面评价,认为微等离子体工艺制备的增材制造材料在力学性能和氧化性能上与变形材料相当。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Development and Characterization of Micro-Plasma Additive Manufacturing Process for Inconel 718 Superalloy
A micro-plasma system was investigated for its capability in additive manufacturing (AM). Micro-plasma AM system has the advantage of lower cost and higher deposition rate over the laser-based AM systems, and generates leaner and cleaner weld deposit than other arc-based AM systems. However, the microplasma system is complex and involves a large number of process variables. In this study, the effects of two arc and wire feed modes on dimensional consistency and hardness were firstly examined. Subsequently, one set of the specimens was further subjected to oxidation tests and the results were compared to that from conventional wrought Inconel 718. It was found that all four processes could produce crack free samples without measurable distortion. Some surface discoloration was observed, ranging from light straw to a purple tint. After heat treatment, the hardness of the samples varies from 403 to 440 HV, with the transverse surface showing slightly lower hardness values. The oxidation tests at 900 °C yielded similar weight change for AM Inconel 718 and its counterpart wrought alloy; however, the rate constant for wrought alloy was slightly higher. Microstructural analysis with SEM and EDS revealed a dendritic structure in the AM Inconel 718 and the presence of Nb-rich compounds in the interdendritic region. The polycrystal grain structure was not delineated in AM material as that in wrought 718. With the increase of exposure time, the oxide layer continues to increase at a higher rate, along with a sublayer of Ni3Nb above the metal substrate. In addition, after 200 hours, the wrought alloy developed porous chromia, while AM material exhibited uneven oxide thickness. In consideration of all aspects of the evaluation carried out thus far, it is concluded that the AM material produced by micro-plasma process is equivalent to wrought material in mechanical properties and oxidation performance.
求助全文
通过发布文献求助,成功后即可免费获取论文全文。 去求助
来源期刊
自引率
0.00%
发文量
0
×
引用
GB/T 7714-2015
复制
MLA
复制
APA
复制
导出至
BibTeX EndNote RefMan NoteFirst NoteExpress
×
提示
您的信息不完整,为了账户安全,请先补充。
现在去补充
×
提示
您因"违规操作"
具体请查看互助需知
我知道了
×
提示
确定
请完成安全验证×
copy
已复制链接
快去分享给好友吧!
我知道了
右上角分享
点击右上角分享
0
联系我们:info@booksci.cn Book学术提供免费学术资源搜索服务,方便国内外学者检索中英文文献。致力于提供最便捷和优质的服务体验。 Copyright © 2023 布克学术 All rights reserved.
京ICP备2023020795号-1
ghs 京公网安备 11010802042870号
Book学术文献互助
Book学术文献互助群
群 号:604180095
Book学术官方微信