伊拉克枣糖浆制备石墨烯的合成与表征

Hasan Hasan Makki, H. H. Alwan
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引用次数: 1

摘要

石墨烯是单层的六方蜂蜜结构的碳原子。以伊枣糖浆为碳源,以浓硫酸为脱水剂,采用膨胀脱水法合成石墨烯。该方法因脱水反应体积增大而得名膨胀脱水。利用FT-IR、XRD、SEM、AFM和UV-Visible等技术对制备的石墨烯进行了表征,并与前人的研究成果进行了比较。最终产物在600℃下退火或热还原,将所有结合结构的氧化基团还原。石墨烯XRD谱图显示出以2θ =23.758°为中心的002面宽峰,d-spacing = 3.37 Å。原子力显微镜图像显示制备的石墨烯以纳米片的形式存在。该方法的产率约为9%,与其他石墨烯制备方法相比,这是相对较高的。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Synthesis and characterization of Graphene produced from Iraqi date syrup
Graphene is a mono layer of hexagonal honey structure of carbon atoms. Iraqi date syrup was used as a carbon source for synthesis Graphene by expanded dehydration method, in which using of concentrated sulfuric acid as dehydration agent. The method name refers to expanded dehydration because of the increasing in volume with dehydration reaction. Characterization the prepared Graphene was done by FT-IR, XRD, SEM, AFM and UV-Visible techniques and compared with previous work. The final product was obtained by annealing at 600 °C or in other word thermal reduction to reduce all oxide groups combined with structure.  Graphene XRD pattern shows wide peak at 002 plane centered at 2θ =23.758°, and d-spacing = 3.37 Å. AFM image shows that prepared Graphene in Nano sheets form. The method exhibit production yield about 9% and this is relatively high in comparison with other Graphene preparation methods.
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