Renata Alves, José Lucio Gonçalves Junior, Daniel Fernandes da Cunha, Kleber de Figueiredo, Geraldo Lúcio de Faria, Wilian da Silva Labiapari
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摘要

. 不锈钢以其在高温下抗腐蚀和抗氧化而闻名。然而,普通铁素体不锈钢通常硬度低,理论上不能通过热处理硬化。虽然铁素体不锈钢4100D (S41003)的化学成分相对简单,重量碳含量仅为0.015%,但以前的研究表明,这种合金可以通过热处理完全或部分硬化。因此,本工作旨在分析不同热处理条件对材料显微组织和硬化的影响。作为一种方法,进行了两种热处理条件,第一种条件是将样品加热到1000℃,分别在5 min、30 min、60 min、120 min和240 min改变奥氏体化时间,然后在水中淬火。在第二种条件下,样品在800℃下进行1 h的临界间退火,然后在烘箱中冷却,然后将样品加热到1000℃,分别在5 min、30 min、60 min、120 min和240 min改变奥氏体化时间,然后在水中淬火。显微组织分析表明,材料在输送状态下呈多边形铁素体结构,析出cr23c6型碳化物,临界间退火处理导致碳化物析出量增加。淬火处理后,定性分析证实了先前的研究表明,由于碳化铬的溶解和晶粒尺寸的增加,马氏体体积率增加。硬化结果表明,该合金在加热至高温时可在水中淬火,且先前退火的材料在淬火时具有更高的硬度。然而,随着奥氏体化时间的延长,硬度降低,奥氏体晶粒尺寸增大。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
MICROESTRUTURA E DUREZA DO AÇO S41003 QUANDO SUBMETIDO A DIFERENTES TRATAMENTOS TÉRMICOS
. Stainless steel is known for its resistance to corrosion and oxidation at high temperatures. However, common ferritic stainless steels generally have low hardness and theoretically are not hardenable by heat treatment. Although ferritic stainless steel 4100D (S41003) has a relatively simple chemical composition, with only 0.015% carbon by weight, previous studies indicate that this alloy can be fully or partially hardened with heat treatment. Therefore, the present work aims to analyze the effect of different heat treatment conditions on the microstructure and hardening of the material. As a methodology, two heat treatment conditions were carried out, in the first condition the samples were heated to 1000 ℃, varying the austenitization time in 5 min, 30 min, 60 min, 120 min and 240 min, then quenched in water. For the second condition, the samples underwent an intercritical annealing at 800 ℃ for 1 h and cooled in the oven, then the samples were heated to 1000 ℃, varying the austenitization time in 5 min, 30 min, 60 min, 120 min and 240 min and quenched in water. The microstructural analysis indicated that the material, in its delivery state, has a polygonal ferritic structure with precipitation of Cr 23 C 6 type carbides, and the intercritical annealing treatment led to an increase in the precipitation of chromium carbide. After the quenching treatment, the qualitative analysis corroborated with previous studies that indicate an increase in the martensite volume rate, due to the dissolution of the chromium carbide and the increase in the grain size. The hardening results indicate that the alloy can be hardened by quenching in water when heated to a high temperature, in addition, the previously annealed material has a higher hardness when quenched. However, with increasing austenitization time, there was a decrease in hardness, associated with an increase in austenitic grain size.
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