基于QuEChERS萃取和气相色谱法分析孟加拉Mymensingh地区当地市场蔬菜中农药残留

M. Alam, R. Hasan, S. Rahman, Md. Abdur Razzak Choudhury, M. Prodhan
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引用次数: 5

摘要

该研究分析了从孟加拉国迈门辛格区5个当地市场采集的两种常见蔬菜(花椰菜和茄子)中的有机磷农药残留。收集到的样本在同一天被送到加齐浦尔孟加拉国农业研究所昆虫学处农药分析实验室。采用快速、简便、廉价、有效、坚固、安全(QuEChERS)提取技术和气相色谱(GC)联用火焰热离子检测器(FTD)对样品进行分析。本研究共分析了60份蔬菜样品。在30份分析的菜花样品中,有5份样品(占样品总数的17%)含有乐果、毒死蜱和喹乐磷残留,其中3份样品的残留超过最大残留限量(MRLs)。在30份茄子样品中,有5份样品(占样品总数的17%)含有毒死蜱、喹乐磷和乐果,其中只有1份样品的残留量超过最大残留限量。本研究反映了Mymensingh地区菜花和茄子中农药残留的实际情况,有助于消费者提高健康和安全意识。因此,应加强对蔬菜中农药残留的持续监测。亚洲Australas。J.食品安全。安全,2022,6 (1),10-17
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Analysis of pesticide residues in vegetables purchased from local markets of Mymensingh district of Bangladesh based on QuEChERS Extraction and Gas Chromatography
The study was conducted to analyze organophosphorus pesticide residues in two common vegetables (cauliflower and eggplant) collected from five local markets of Mymensingh district of Bangladesh. The collected samples were carried to the Pesticide Analytical Laboratory, Entomology Division of Bangladesh Agricultural Research Institute (BARI), Gazipur on the same sampling day. The collected samples were analyzed using Quick, Easy, Cheap, Effective, Rugged and Safe (QuEChERS) extraction technique and Gas Chromatography (GC) coupled with Flame Thermionic Detector (FTD). In total, 60 vegetable samples were analyzed in this study. Out of 30 analyzed samples of cauliflower, 5 samples (17% of the total number of samples) contained residues of dimethoate, chlorpyrifos and quinalphos, where 3 samples contained residues above the maximum residue limits (MRLs). Among the 30 analyzed samples of eggplant, 5 samples (17% of the total number of samples) contained residues of chlorpyrifos, quinalphos, and dimethoate, where only one sample contained residues above MRL. This study reflects the actual scenario of pesticide residues remain in cauliflower and eggplant collected from local markets of Mymensingh district, which will help the consumer to be aware of their health and safety. Thus, continuous monitoring of pesticide residues in vegetables should be strengthened. Asian Australas. J. Food Saf. Secur. 2022, 6 (1), 10-17
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