263 GHz动态核极化回旋管的演示

M. Blank, P. Borchard, P. Cahalan, S. Cauffman, K. Felch, M. Rosay, L. Tometich
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引用次数: 9

摘要

动态核极化(DNP)通过将未成对电子自旋的高极化转移到核自旋上来提高核磁共振实验的灵敏度。极化转移是由高频毫米波辐照驱动的。通信和电力工业公司是Bruker Biospin公司263 GHz DNP光谱仪回旋管的原始设备制造商,该光谱仪与400 MHz核磁共振系统一起使用。DNP系统的关键部件包括一个工作在263ghz附近、功率水平为25w的连续波回旋管、一个9.7 T超导磁体、一个电源和控制系统、一个从回旋管到核磁共振样品的传输线和一个低温磁角旋转探针。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Demonstration of a 263 GHz gyrotron for Dynamic Nuclear Polarization
Dynamic Nuclear Polarization (DNP) can be used to increase the sensitivity of nuclear magnetic resonance (NMR) experiments by transferring the much higher polarization of unpaired electrons spins to nuclear spins. The polarization transfer is driven by high frequency millimeter wave irradiation. Communications and Power Industries is an original equipment manufacturer of gyrotron tubes for Bruker Biospin's 263 GHz DNP spectrometer, which is used with a 400 MHz NMR system. The key components of the DNP system include a cw gyrotron tube operating near 263 GHz at power levels of 25 W, nominally, a 9.7 T superconducting magnet, a power supply and control system, a transmission line from the gyrotron to the NMR sample, and a low-temperature magnetic-angle-spinning probe.
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