单源前驱体法制备硒化铜和硒化铟纳米颗粒

Proceedings of 2013 10th International Bhurban Conference on Applied Sciences & Technology (IBCAST) Pub Date : 2013-05-02 DOI:10.1109/IBCAST.2013.6512127

S. N. Malik, H. Ahmed, M. Shahid, N. Haider, M. Malik, P. O’Brien

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引用次数: 3

摘要

采用金属与配体盐[HNEt3][iPr2PSe2]的复分解反应合成了Mx(iPr2PSe2)y]配合物(M = In, Cu)。这些配合物在200-270°C的HDA/TOP中进行热裂解，得到单相Cu2-xSe和In2Se3纳米颗粒。在250℃下生长的Cu2-xSe纳米粒子和在270℃下生长的In2Se3纳米粒子的平均直径分别为5.0±1.2 nm和13±2.5 nm。

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Colloidal preparation of copper selenide and indium selenide nanoparticles by single source precursors approach

M_x(ⁱPr₂PSe₂)_y] complexes (M = In, Cu) were synthesized by metathesis reaction of metal with ligand salt [HNEt₃][ⁱPr₂PSe₂]. These complexes undergo thermolysis in HDA/TOP at 200-270 °C, to yield monophasic Cu_2-xSe and In₂Se₃ nanoparticles. Cu_2-xSe nanoparticles (grown at 250 °C) and In₂Se₃ nanoparticles (grown at 270 °C) had a mean diameter of 5.0 ± 1.2 nm and 13 ± 2.5 nm, respectively.

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Proceedings of 2013 10th International Bhurban Conference on Applied Sciences & Technology (IBCAST)

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