C. Lopez, D. Meyers, A. Saddawi, A. Saveliev, K. Brezinsky
{"title":"等离子体辅助合成碳化钼催化剂","authors":"C. Lopez, D. Meyers, A. Saddawi, A. Saveliev, K. Brezinsky","doi":"10.5210/JUR.V2I1.7463","DOIUrl":null,"url":null,"abstract":"A novel method for the production of a nano-structured molybdenum carbide catalyst using non-thermal plasma is described. This synthesis involves the carburization of a molybdenum metal powder precursor using ethylene as the carbon source. Transmission electron microscopy (TEM) showed the presence of a Mo 2 C-β crystal structure and a 9 � 2 nm layer of what was suspected to be Mo 2 C absent in the molybdenum precursor. Catalytic testing in the water gas shift reaction (WGS) showed no difference in activity between the unreduced synthesis product and the control run.","PeriodicalId":426348,"journal":{"name":"The Journal of Undergraduate Research at the University of Illinois at Chicago","volume":"40 1","pages":"0"},"PeriodicalIF":0.0000,"publicationDate":"2008-10-24","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":"{\"title\":\"Plasma Assisted Synthesis of a Molybdenum Carbide Catalyst\",\"authors\":\"C. Lopez, D. Meyers, A. Saddawi, A. Saveliev, K. Brezinsky\",\"doi\":\"10.5210/JUR.V2I1.7463\",\"DOIUrl\":null,\"url\":null,\"abstract\":\"A novel method for the production of a nano-structured molybdenum carbide catalyst using non-thermal plasma is described. This synthesis involves the carburization of a molybdenum metal powder precursor using ethylene as the carbon source. Transmission electron microscopy (TEM) showed the presence of a Mo 2 C-β crystal structure and a 9 � 2 nm layer of what was suspected to be Mo 2 C absent in the molybdenum precursor. Catalytic testing in the water gas shift reaction (WGS) showed no difference in activity between the unreduced synthesis product and the control run.\",\"PeriodicalId\":426348,\"journal\":{\"name\":\"The Journal of Undergraduate Research at the University of Illinois at Chicago\",\"volume\":\"40 1\",\"pages\":\"0\"},\"PeriodicalIF\":0.0000,\"publicationDate\":\"2008-10-24\",\"publicationTypes\":\"Journal Article\",\"fieldsOfStudy\":null,\"isOpenAccess\":false,\"openAccessPdf\":\"\",\"citationCount\":\"0\",\"resultStr\":null,\"platform\":\"Semanticscholar\",\"paperid\":null,\"PeriodicalName\":\"The Journal of Undergraduate Research at the University of Illinois at Chicago\",\"FirstCategoryId\":\"1085\",\"ListUrlMain\":\"https://doi.org/10.5210/JUR.V2I1.7463\",\"RegionNum\":0,\"RegionCategory\":null,\"ArticlePicture\":[],\"TitleCN\":null,\"AbstractTextCN\":null,\"PMCID\":null,\"EPubDate\":\"\",\"PubModel\":\"\",\"JCR\":\"\",\"JCRName\":\"\",\"Score\":null,\"Total\":0}","platform":"Semanticscholar","paperid":null,"PeriodicalName":"The Journal of Undergraduate Research at the University of Illinois at Chicago","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.5210/JUR.V2I1.7463","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
Plasma Assisted Synthesis of a Molybdenum Carbide Catalyst
A novel method for the production of a nano-structured molybdenum carbide catalyst using non-thermal plasma is described. This synthesis involves the carburization of a molybdenum metal powder precursor using ethylene as the carbon source. Transmission electron microscopy (TEM) showed the presence of a Mo 2 C-β crystal structure and a 9 � 2 nm layer of what was suspected to be Mo 2 C absent in the molybdenum precursor. Catalytic testing in the water gas shift reaction (WGS) showed no difference in activity between the unreduced synthesis product and the control run.