纳米lifepo4电池材料的制备及性能研究

Yajun Mao
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引用次数: 1

摘要

本研究采用不同工艺制备了纳米lifepo4作为锂电池正极材料,并对其微观形貌、晶体结构和电化学性能进行了测试。采用高温固相法和凝胶-溶胶法制备磷酸铁锂。用电子显微镜观察了产物的微观形貌。用X衍射仪检测产物的晶体结构。通过充放电测试了产品的电化学性能。结果表明:凝胶-溶胶法制备的磷酸铁锂具有粒径更小、形状更规则的特点;两种磷酸铁锂的衍射模式基本一致,但凝胶-溶胶法制备的磷酸铁锂由于粒径较小,衍射强度较小;凝胶-溶胶法制备的磷酸铁锂更加稳定高效,充放电容量更大。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
Preparation and properties of battery material nano-LiFePO4

In this study, nano-LiFePO4 as the cathode material of lithium battery was prepared by different processes, and its micromorphology, crystal structure, and electrochemical performance were tested. Lithium iron phosphate was prepared by the high-temperature solid-state method and gel–sol method. The micro morphology of the product was detected by an electron microscope. The crystal structure of the product was detected by an X diffractometer. The electrochemical performance of the product was tested by charge and discharge. The results showed that the lithium iron phosphate prepared by the gel–sol method had a smaller particle size and more regular shape; the diffraction pattern of the two kinds of lithium iron phosphate was nearly consistent, but the lithium iron phosphate prepared by the gel–sol method had smaller diffraction intensity because of its smaller particle size; the lithium iron phosphate prepared by the gel–sol method were more stable and efficient and had a larger capacity during charging and discharging.

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