Denis Mettus, Alfonso Chacon, Andreas Bauer, Sebastian Mühlbauer, Christian Pfleiderer
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Optimization strategies and artifacts of time-involved small-angle neutron scattering experiments.
Kinetic small-angle neutron scattering provides access to the microscopic properties of mesoscale systems under slow, periodic perturbations. By interlocking the phases of neutron pulse, sample modulation and detector signal, time-involved small-angle neutron scattering experiments (TISANE) allow one to exploit the neutron velocity spread and record data without major sacrifice in intensity at timescales down to microseconds. This article reviews the optimization strategies of TISANE that arise from specific aspects of the process of data acquisition and data analysis starting from the basic principles of operation. Typical artifacts of data recorded in TISANE due to the choice of time binning and neutron chopper pulse width are illustrated by virtue of the response of the skyrmion lattice in MnSi under periodic changes of the direction of the stabilizing magnetic field.
期刊介绍:
Many research topics in condensed matter research, materials science and the life sciences make use of crystallographic methods to study crystalline and non-crystalline matter with neutrons, X-rays and electrons. Articles published in the Journal of Applied Crystallography focus on these methods and their use in identifying structural and diffusion-controlled phase transformations, structure-property relationships, structural changes of defects, interfaces and surfaces, etc. Developments of instrumentation and crystallographic apparatus, theory and interpretation, numerical analysis and other related subjects are also covered. The journal is the primary place where crystallographic computer program information is published.