Mechanical properties of bulk-fill resin composites with single increment up to 4 mm: A novel mechanical strength test.

Abstract

Purpose: To evaluate the mechanical properties of two brands of bulk-fill resin composites placed in a single increment up to 4 mm thickness via a novel mechanical strength test and provide related explanations.

Methods: Light transmission (LT), translucency parameter (TP), color difference (ΔE), Vickers hardness (HV) of two bulk-fill resin composites (Filtek Bulk Fill Posterior, Tetric N-Ceram Bulk Fill) and two conventional resin composites (Z100, Spectrum TPH) were evaluated. A novel flexural strength (FS) test method was applied for bulk-fill resin composite to determine the FS value of the bottom composites at depths of 1, 2, 3, and 4 mm after 24 hours of aging treatment (3 months water storage and 15,000 thermal cycles). The conventional resin composites were also tested for FS and all the FS results were subjected to Weibull analysis. Degree of conversion (DC) in the bulk-fill resin composites, light-cured at depths of 1, 2, 3, and 4 mm and conventional resin composites at depths of 2 and 4 mm, were assessed by FTIR.

Results: Both bulk-fill resin composites showed higher light transmission and translucency than that of conventional ones at each of the same thicknesses (1, 2, 3, 4 mm), wherein their flexural strength was not affected by depth. The Weibull analysis suggested both bulk-fill resin composites achieved good reliability and structural integrity under each curing thickness. Vickers hardness was affected by the material type and thickness. Bulk-fill resin composites showed a decrease in degree of conversion between 1 mm and 4 mm, but both were over 55%.

Clinical significance: Filtek Bulk Fill Posterior, Tetric N-Ceram Bulk Fill achieved acceptable mechanical properties when cured at depths of up to 4 mm, which was beneficial from their optical and polymerized properties.