{"title":"preparation of palladium Catalyst from bauxite ore and using for kerosene treatment","authors":"W. Saeed, Qaidar Salim","doi":"10.33899/EDUSJ.2020.127951.1103","DOIUrl":null,"url":null,"abstract":"The research was aimed to used bauxite ore that has a high aluminum minerals which available in AlHussainiyat near al-Anbar district as a source of alumina which it used as a catalyst support after being loaded with palladium metal , The components of both bauxite ore and prepared catalyst were studied by X-ray diffraction and fluorescence as well as thermogravimetric analysis (TGA) of the prepared catalyst , After this the catalyst was used in the treatment of kerosene which is distilled at (150-260C) under different conditions of the (temperature , reaction time and the ratio of catalyst) to know the optimal reaction conditions that determid by measuring the (FTIR) and chemical analysis. The optimal conditions: temperature was (250C), reaction time was (2hours) and the catalyst ratio was (2%) .The catalyst appeard the ability to dehydrogenation reaction and reforming to form olefinic and aromatic compounds. The research also included the study of n-paraffins separated from kerosene samples that were treating in different temperatures (150,200,250C ) using (HNMR).The results showed the ability of the catalyst towards catalytic cracking and converting n-paraffins to iso-paraffins .","PeriodicalId":15610,"journal":{"name":"Journal of Education Science","volume":"30 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"2020-09-21","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Journal of Education Science","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.33899/EDUSJ.2020.127951.1103","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
The research was aimed to used bauxite ore that has a high aluminum minerals which available in AlHussainiyat near al-Anbar district as a source of alumina which it used as a catalyst support after being loaded with palladium metal , The components of both bauxite ore and prepared catalyst were studied by X-ray diffraction and fluorescence as well as thermogravimetric analysis (TGA) of the prepared catalyst , After this the catalyst was used in the treatment of kerosene which is distilled at (150-260C) under different conditions of the (temperature , reaction time and the ratio of catalyst) to know the optimal reaction conditions that determid by measuring the (FTIR) and chemical analysis. The optimal conditions: temperature was (250C), reaction time was (2hours) and the catalyst ratio was (2%) .The catalyst appeard the ability to dehydrogenation reaction and reforming to form olefinic and aromatic compounds. The research also included the study of n-paraffins separated from kerosene samples that were treating in different temperatures (150,200,250C ) using (HNMR).The results showed the ability of the catalyst towards catalytic cracking and converting n-paraffins to iso-paraffins .