Calibration bath uncertainty in precision temperature measurements

Abstract

Calibration baths are widely used in many laboratories worldwide for the calibration of thermometers by comparison. They come in different shapes and sizes and use different media (water, alcohol, silicon oil etc.), but a certain nonuniformity of theused media is always present. During precision temperature measurements, uniformity (homogeneity and temporal stability) of a calibration bath is of the utmost importance since its contribution to total measurement uncertainty is the largest. The temperature gradient can be described as a change of temperature at different positions inside the bath working volume. Temporal temperature stability depends on many factors such as: the bath temperature, control system, bath construction and the flow of the used media inside the bath, just to name a few. In this paper, we investigate uniformity of a cylindrical calibration bath. Homogeneity is determined by measurement of axial and radial temperature gradient inside the bath. Stability is examined by observation of the change in temperature reading during certain period of time. The obtained results are compared with manufacturer specification and can be used for determination of calibration bath contribution to total measurement uncertainty during calibration of thermometers.