Nanoscratch Property of Self-lubricating Ti/MoS2 Nanocoating at Nano-scale Level

Summèra Banday, M. F. Wani, M. Mir, J. Singh, S. Mushtaq, Jebran Khan, S. S. Saleem
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引用次数: 2

Abstract

Nanoscratch test was performed on self-lubricating Ti/MoS2 coating of 99.79 nm thickness prepared by pulse laser deposited technique on Al-13Si substrate. The surface morphology and surface elemental analysis of Ti/MoS2 were studied using Scanning electron microscope integrated with Energy dispersive X-ray spectroscopy. The structural analysis of Ti/MoS2 coating was conducted using X-ray diffraction and Raman spectroscopy. Nanoscratch tests were carried out at low load of 250-1250 µN to examine the deformation and failure behaviour of the coating/substrate system. The results indicate that Ti/MoS2 coating show better adhesion strength at low loads. Also, in-situ scanning probe microscope images of Ti/MoS2 coating shows plastic flow of coating with no debris and cracks on the surface. Thus, the mode of wear mechanism is mainly ductile and abrasive.
纳米级自润滑Ti/MoS2纳米涂层的纳米划痕性能
采用脉冲激光沉积技术在Al-13Si衬底上制备了厚度为99.79 nm的自润滑Ti/MoS2涂层,并进行了纳米划痕实验。利用扫描电镜结合能量色散x射线能谱技术研究了Ti/MoS2的表面形貌和表面元素分析。利用x射线衍射和拉曼光谱对Ti/MoS2涂层进行了结构分析。在250-1250µN的低载荷下进行纳米划伤试验,以检查涂层/基体系统的变形和破坏行为。结果表明,Ti/MoS2涂层在低负荷下具有较好的附着强度。Ti/MoS2涂层的原位扫描探针图像显示涂层的塑性流动,表面无碎屑和裂纹。因此,磨损机制的模式主要是韧性和磨料。
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