Effect of heat treatments on microstructure and mechanical properties of Al0.5CoCrFeNi complex concentrated alloy

J. Lapin, M. Makwana, A. Klimová
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引用次数: 2

Abstract

The effect of heat treatments on microstructure and mechanical properties of Al0.5CoCr FeNi complex concentrated alloy (CCA) was studied. The CCA was prepared by vacuum induction melting of pure elements and solidification in ceramic crucibles. The as-solidified alloy was subjected to heat treatments consisting of solid solution annealing, water quenching and precipitation hardening. The microstructure of the as-solidified alloy consists of fcc(A1) dendrites and an interdendritic region composed of bcc(B2), bcc(A2) and fcc(A1) phases. The solution annealing followed by water quenching and ageing at 800 and 900◦C leads to the precipitation of needle-like bcc(B2) particles in fcc(A1) dendrites and the formation of the interdendritic region composed of bcc(B2) and fcc(A1) phases. The volume fraction of needle-like bcc(B2) precipitates increases with increasing ageing time and decreasing ageing temperature. The size of bcc(B2) precipitates increases with increasing ageing time and ageing temperature. Vickers microhardness, Vickers hardness and room temperature yield strength of the heat-treated alloy increase with decreasing ageing temperature and increasing ageing time up to 5 h and then decrease at a longer ageing time up to 25 h. K e y w o r d s: complex concentrated alloys, precipitation hardening, heat treatment, microstructure, mechanical properties
热处理对Al0.5CoCrFeNi复合浓缩合金组织和力学性能的影响
研究了热处理对Al0.5CoCr FeNi复合浓缩合金(CCA)显微组织和力学性能的影响。采用真空感应熔炼纯元素,在陶瓷坩埚中凝固法制备了CCA。对凝固态合金进行固溶退火、水淬和沉淀硬化等热处理。凝固态合金的显微组织由fcc(A1)枝晶和bcc(B2)、bcc(A2)和fcc(A1)相组成的枝晶间区组成。固溶退火后再进行800℃和900℃的水淬时效处理,fcc(A1)枝晶中析出针状bcc(B2)颗粒,并形成由bcc(B2)和fcc(A1)相组成的枝晶间区。针状bcc(B2)相体积分数随时效时间的延长和时效温度的降低而增大。随着时效时间和时效温度的增加,bcc(B2)析出物的尺寸增大。热处理合金的维氏显微硬度、维氏硬度和室温屈服强度随时效温度的降低和时效时间的延长而增大,时效时间可达5 h,时效时间越长,时效时间可达25 h,合金的显微硬度、维氏硬度和室温屈服强度越低
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