To study the synthesis mechanism and structural properties of nickel doped SnO2 nanostructured materials with variation of dopant concentration

Sonia Arora, Rajesh Sharma
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Abstract

Nanocomposites are those materials which contain multiple domains with the combination of two or more different materials and possessing minimum one phase domain lying in the nanometer range (1nm-100nm). Nanocomposites materials possess so many novel and challenging properties. In present work, nanocomposites of tin oxide doped with nickel oxide were synthesized by simple chemical route method via co precipitation method. Various characterization techniques were employed to characterize the as-synthesized and calcined samples of Ni doped SnO2 nanostructured materials using diffraction by X-ray analysis, Fourier infrared spectroscopy (IR). The crystallite size of samples is determined by using Debye Scherer formulation and with considering the most intense peak. The FTIR spectrograph reveals that different peaks of metal oxides correspond to SnO2 and NiO were present in samples.
研究不同掺杂浓度下镍掺杂SnO2纳米结构材料的合成机理和结构性能
纳米复合材料是由两种或两种以上不同的材料组合而成的具有多个畴的材料,并且在纳米范围(1nm-100nm)内具有最小一个相畴。纳米复合材料具有许多新颖和具有挑战性的性能。本文采用共沉淀法,采用简单的化学路线合成了氧化锡掺杂氧化镍的纳米复合材料。利用衍射、x射线分析、傅立叶红外光谱(IR)等多种表征技术对Ni掺杂SnO2纳米结构材料的合成和煅烧样品进行了表征。样品的晶粒尺寸采用Debye - Scherer公式,考虑最强峰。红外光谱分析表明,样品中存在与SnO2和NiO相对应的不同金属氧化物峰。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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