Preliminary study on the synthesis of granular ordered mesoporous carbon–montmorillonite composite adsorbents for removal of water pollutants

M. A. Zulkifli, A. Afandi, A. M. Din
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引用次数: 2

Abstract

In this preliminary work, ordered mesoporous carbon–montmorillonite (OMC–M) composite granules were synthesised and tested for the removal of methylene blue and methyl red. The synthesised OMC–M composite granules were characterised using a scanning electron microscope (SEM), an energy dispersive x-ray spectroscope (EDX), and a Brunauer-Emmett-Teller (BET) surface analyser. The OMC–M composite granules were bound using polyvinyl alcohol (PVA) as a binding agent. The swelling/burst effect of the composite granules in distilled water was investigated using different PVA concentrations, ranging from 1% to 5% (w/v) at different observation times of up to 24 hours. The results indicated that there were no significant changes on the average area (1.85 mm) of the OMC–M composite granules when the PVA binder concentration was increased. OMC–M composite granules with 5% (w/v) PVA displayed removal efficiency of 85% and 65% for methylene blue and methyl red, respectively. The results of this study suggested the potential of applying OMC–M composite granules for the removal of various pollutants from an aqueous solution.In this preliminary work, ordered mesoporous carbon–montmorillonite (OMC–M) composite granules were synthesised and tested for the removal of methylene blue and methyl red. The synthesised OMC–M composite granules were characterised using a scanning electron microscope (SEM), an energy dispersive x-ray spectroscope (EDX), and a Brunauer-Emmett-Teller (BET) surface analyser. The OMC–M composite granules were bound using polyvinyl alcohol (PVA) as a binding agent. The swelling/burst effect of the composite granules in distilled water was investigated using different PVA concentrations, ranging from 1% to 5% (w/v) at different observation times of up to 24 hours. The results indicated that there were no significant changes on the average area (1.85 mm) of the OMC–M composite granules when the PVA binder concentration was increased. OMC–M composite granules with 5% (w/v) PVA displayed removal efficiency of 85% and 65% for methylene blue and methyl red, respectively. The results of this study suggested the pot...
颗粒状有序介孔碳-蒙脱土复合吸附剂的合成及其对水污染物的去除效果初步研究
在这项初步工作中,合成了有序介孔碳-蒙脱土(OMC-M)复合颗粒,并对其去除亚甲基蓝和甲基红进行了测试。利用扫描电子显微镜(SEM)、能量色散x射线光谱仪(EDX)和布鲁诺尔-埃米特-泰勒(BET)表面分析仪对合成的OMC-M复合颗粒进行了表征。以聚乙烯醇(PVA)为粘结剂,对OMC-M复合颗粒进行了粘结。研究了不同PVA浓度(1% ~ 5% w/v)下复合颗粒在蒸馏水中的膨胀/破裂效应,观察时间最长为24小时。结果表明,随着PVA黏合剂浓度的增加,OMC-M复合颗粒的平均面积(1.85 mm)没有明显变化。5% (w/v) PVA的OMC-M复合颗粒对亚甲基蓝和甲基红的去除率分别为85%和65%。本研究的结果表明,应用OMC-M复合颗粒去除水溶液中各种污染物的潜力。在这项初步工作中,合成了有序介孔碳-蒙脱土(OMC-M)复合颗粒,并对其去除亚甲基蓝和甲基红进行了测试。利用扫描电子显微镜(SEM)、能量色散x射线光谱仪(EDX)和布鲁诺尔-埃米特-泰勒(BET)表面分析仪对合成的OMC-M复合颗粒进行了表征。以聚乙烯醇(PVA)为粘结剂,对OMC-M复合颗粒进行了粘结。研究了不同PVA浓度(1% ~ 5% w/v)下复合颗粒在蒸馏水中的膨胀/破裂效应,观察时间最长为24小时。结果表明,随着PVA黏合剂浓度的增加,OMC-M复合颗粒的平均面积(1.85 mm)没有明显变化。5% (w/v) PVA的OMC-M复合颗粒对亚甲基蓝和甲基红的去除率分别为85%和65%。这项研究的结果表明……
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