R. Nicula, V. Cojocaru, J. Bednarčík, M. Stir, E. Burkel
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引用次数: 1
Abstract
The properties of nanocrystalline materials differ from the ones of their coarse- grained counterparts. Significant changes of the phase diagrams were also recently reported for various nanomaterials. Thermomechanical processing routes - with or without pressure application - employed to obtain bulk nanostructured solids from nanocrystalline powders control the microstructural features down to the nanoscale and thus determine the final nanomaterial properties. Modern in-situ X-ray diffraction experiments provide effective tools for the observation and engineering of the microstructure in nanomaterials. Time-resolved in-situ synchrotron radiation diffraction experiments were here used to monitor the evolution of the weighted column-length distributions and microstrain at specimen-relevant scales during heating of nanocrystalline HITPERM and NANOPERM alloys. Diffraction line pro- file analysis methods were applied to observe the grain growth kinetics in these Fe(Co)-Zr- B-Cu nanostructured alloys. The retention of their excellent soft magnetic properties in par- ticular at high temperature depends on the ability to supress anomalous grain growth.
期刊介绍:
Zeitschrift für Kristallographie International journal for structural, physical, and chemical aspects of crystalline materials ISSN 0044-2968 Founded in 1877 by Paul Groth Zeitschrift für Kristallographie is one of the world’s oldest scientific journals. In original papers, letters and review articles it presents results of theoretical or experimental study on crystallography.