P. K. Byers, A. Canty, Hong Jin, D. Kruis, B. A. Markies, J. Boersma, G. Koten, Geoffrey S. Hill, M. J. Irwin, L. Rendina, R. Puddephatt
{"title":"Dimethylpalladium(II) and Monomethylpalladium(II) Reagents and Complexes","authors":"P. K. Byers, A. Canty, Hong Jin, D. Kruis, B. A. Markies, J. Boersma, G. Koten, Geoffrey S. Hill, M. J. Irwin, L. Rendina, R. Puddephatt","doi":"10.1002/9780470132630.CH28","DOIUrl":null,"url":null,"abstract":"Syntheses of organopalladium(II) reagents containing N,N,N',N'-tetramethylethylenediamine (tmeda), pyridazine, dimethylsulfide, 2,2'-bipyridine (bpy), triphenylphosphine and bis(1,1'-diphenylphosphino)ferrocene (dppf) are described, together with trans-dichlorobis(dimethylsulfide)palladium(II) and trans-dibromobis(dimethylsulfide)palladium(II). Syntheses are described for dimethyl(pyridazine)palladium(II), monomethylpalladium(II) complexes of dimethylsulfide, [PdMe(SMe2)(mu-X)]2 (X = Cl, Br, I), PdMe2(tmeda) and PdXMe(tmeda) (X = Cl, Br, I), PdMe2(dppf) and PdXMe(dppf) (X = Cl, Br, I), cis-PdMe2(PPh3)2 and trans-PdClMe(PPh3)2 (X = Cl, Br, I), and trans-PdXMe(bpy) (X = Cl, Br, I).","PeriodicalId":13689,"journal":{"name":"Inorganic Syntheses","volume":"39 1","pages":"162-172"},"PeriodicalIF":0.0000,"publicationDate":"1998-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"28","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Inorganic Syntheses","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.1002/9780470132630.CH28","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 28
Abstract
Syntheses of organopalladium(II) reagents containing N,N,N',N'-tetramethylethylenediamine (tmeda), pyridazine, dimethylsulfide, 2,2'-bipyridine (bpy), triphenylphosphine and bis(1,1'-diphenylphosphino)ferrocene (dppf) are described, together with trans-dichlorobis(dimethylsulfide)palladium(II) and trans-dibromobis(dimethylsulfide)palladium(II). Syntheses are described for dimethyl(pyridazine)palladium(II), monomethylpalladium(II) complexes of dimethylsulfide, [PdMe(SMe2)(mu-X)]2 (X = Cl, Br, I), PdMe2(tmeda) and PdXMe(tmeda) (X = Cl, Br, I), PdMe2(dppf) and PdXMe(dppf) (X = Cl, Br, I), cis-PdMe2(PPh3)2 and trans-PdClMe(PPh3)2 (X = Cl, Br, I), and trans-PdXMe(bpy) (X = Cl, Br, I).
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