Optimization of Reduction Process of Egyptian Ilmenitevia Metallothermic reactions

A. Daher, N. Badawy, W. Mohrez, AbdAllh M. Abd El-Hamid, A. Yossef, A. A. El, Pasir
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Abstract

It is important to develop technologies for the production of master alloys for industrial applications. Detailed research on reduction of titanium from Egyptian ilmenite by an aluminothermic process in a graphite Crucible was charged by the mixture of ilmenite, flux, aluminum was investigated. This paper study the effect of aluminum feed (10%35%), flux material (type, and amount), and temperature preheat from 50 C to 400 C and time of preheating from 0.5 hr. to 3 hrs. Then, the metallic samples formed by the reduction were analyzed using X-ray diffraction, scanning electron microscopy. The mixed fluxes were strongly and successfully reduced ilmenite to a high-purity master alloy with small amounts of detected impurities.
利用金属热反应优化埃及钛矿还原工艺
开发工业用母合金的生产技术是十分重要的。以钛铁矿、助熔剂、铝为原料,在石墨坩埚中用铝热法从埃及钛铁矿中还原钛。本文研究了铝料(10% ~ 35%)、助熔剂材料(种类、用量)、预热温度为50℃~ 400℃,预热时间为0.5 h的影响。到3小时。然后用x射线衍射、扫描电镜对还原后的金属样品进行分析。混合助熔剂强烈而成功地将钛铁矿还原为具有少量检测杂质的高纯度母合金。
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