1.2.4. Synthesis, crystal structure and thermal stability property of Ni(aze)(4,4′ –bipy)(H2O) based on longer-spanning azelaic acid and 4,4′ -bipyridine ligands
{"title":"1.2.4. Synthesis, crystal structure and thermal stability property of Ni(aze)(4,4′ –bipy)(H2O) based on longer-spanning azelaic acid and 4,4′ -bipyridine ligands","authors":"G. Song, F. Bai, Yan Xie, Y. Xing","doi":"10.21060/CIS.V1I2.2000","DOIUrl":null,"url":null,"abstract":"Abstract: One new three-dimensional (3D) supramolecular longer-spanning azelaic acid (H 2 aze) complex: Ni(aze)(4,4 ′ – bipy)(H 2 O) (4,4 ′ -bipy = 4,4 ′ -bipyridine) has been synthesized using hydrothermal conditions and characterized by elemental analysis, IR spectroscopy, UV spectrum, powder X-ray diffraction, TG analysis and single crystal X–ray diffraction. Structural analysis reveals that the title complex is six-coordinate and connected by the azelaic acid and 4,4 ′ -bipy ligands to generate a 2D planar structure, further linked through the interaction of hydrogen bond of C–H···O to form a 3D supramolecular structure . Supporting information: FT-IR, UV-Vis, X-Ray, Cif file","PeriodicalId":10648,"journal":{"name":"Communications in Inorganic Synthesis","volume":"1 1","pages":""},"PeriodicalIF":0.0000,"publicationDate":"1900-01-01","publicationTypes":"Journal Article","fieldsOfStudy":null,"isOpenAccess":false,"openAccessPdf":"","citationCount":"0","resultStr":null,"platform":"Semanticscholar","paperid":null,"PeriodicalName":"Communications in Inorganic Synthesis","FirstCategoryId":"1085","ListUrlMain":"https://doi.org/10.21060/CIS.V1I2.2000","RegionNum":0,"RegionCategory":null,"ArticlePicture":[],"TitleCN":null,"AbstractTextCN":null,"PMCID":null,"EPubDate":"","PubModel":"","JCR":"","JCRName":"","Score":null,"Total":0}
引用次数: 0
Abstract
Abstract: One new three-dimensional (3D) supramolecular longer-spanning azelaic acid (H 2 aze) complex: Ni(aze)(4,4 ′ – bipy)(H 2 O) (4,4 ′ -bipy = 4,4 ′ -bipyridine) has been synthesized using hydrothermal conditions and characterized by elemental analysis, IR spectroscopy, UV spectrum, powder X-ray diffraction, TG analysis and single crystal X–ray diffraction. Structural analysis reveals that the title complex is six-coordinate and connected by the azelaic acid and 4,4 ′ -bipy ligands to generate a 2D planar structure, further linked through the interaction of hydrogen bond of C–H···O to form a 3D supramolecular structure . Supporting information: FT-IR, UV-Vis, X-Ray, Cif file
求助内容：
应助结果提醒方式：
京公网安备 11010802042870号
