Study of Structural and Optical Properties of Fe2+ Doped Tin Oxide Nanoparticles

K. Reddy, S. Nithiyanantham, G. Geetha, R. Sujatha, S. Mahalakshmi
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引用次数: 5

Abstract

Tin dioxide nanoparticles (SnO2) were synthesized by a sol-gel method. And tin tetra chloride (SnCl4) and ammonium hydroxide (NH4OH) were used as the precursor. NH4OH maintain the homogeneity and stoichiometry of solution through pH. The obtained powder subjected to calcination about 110oC. The obtained samples are characterized by X-ray diffraction, Scanning electron microscope, Fourier transform infrared spectroscope and UV-Visible spectroscopy. From the characterizations it is confirmed that the tetragonal structure and the particles are small and nanosizes, The O-H stretching and C=C bending stretching with chemical compositions are analyzed. The improved conduction properties through lower bandgap and the results are further interpreted and discussed.
Fe2+掺杂氧化锡纳米颗粒的结构和光学性质研究
采用溶胶-凝胶法制备了二氧化锡纳米颗粒。以四氯化锡(SnCl4)和氢氧化铵(NH4OH)为前驱体。NH4OH通过ph保持溶液的均匀性和化学计量性。所得粉体经过110℃左右的煅烧。采用x射线衍射、扫描电镜、傅里叶变换红外光谱和紫外可见光谱对所得样品进行了表征。通过表征,证实了该材料的四边形结构和颗粒尺寸均为纳米级,并分析了O-H拉伸和C=C弯曲拉伸的化学成分。进一步解释和讨论了低带隙对导电性能的改善。
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