Additive manufacturing of an Fe–Cr–Co permanent magnet alloy with a novel approach of in-situ alloying

S. Arneitz, R. Buzolin, S. Rivoirard, C. Sommitsch
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引用次数: 1

Abstract

Abstract Additive manufacturing has become increasingly important in the production of magnetic materials in recent years due to the great demands for miniaturization and complex-shaped magnet parts. In this study, the laser beam-powder bed fusion process (LPBF) has been used to develop an in-situ alloying process for the additive manufacturing of a permanent magnet material of the Fe–Cr–Co system. This novel method allows for the production of complex alloys with a chemical composition suited to each specific case of application, achieved by using elemental powders or simpler commercial alloy powders as base materials. The core focus of this study has been on the development and characterization of the printing process using a Fe-30.5Cr-15Co-1.5Mo alloy. The in-situ alloying process has been developed by performing melt pool tests on the two main component powders Fe and Cr and by conducting parameter studies using two different powder mixtures with different sphericity of their components. The influence of different printing parameters and post-printing treatments on the chemical homogeneity and magnetic properties has been studied for selected samples. In addition, magnetic measurements at different temperatures have been performed to investigate the temperature stability of the magnetic properties of the 3D printed material. Impact Statement As by today, the current amount of research done on the additive manufacturing of magnetic materials is rather low. Most of research is focused on rare- earth containing magnetic materials. In this work therefore, we are taking another direction in which we will show that LPBF combined with in- situ alloying is an ideal method for the production of a great variety of different rare- earth free magnetic materials. The positive results of our work can both have an influence on the the scientific community, as further research in the field on different promising rare- earth free magnetic materials is to be expected. Furthermore, a positiv economic impact may occur since the production of rare- earth free magnetic materials is dependent on different raw material sources which are both more cost- effectiv and less critical in terms of their supply chain. This effect is also accompanied by a positive environmental impact, since the mining of rare- earth metals usually comes with considerable environmental pollution.
采用原位合金化新方法制备Fe-Cr-Co永磁合金
近年来,由于对磁性零件小型化和形状复杂的要求越来越高,增材制造在磁性材料的生产中变得越来越重要。在本研究中,采用激光束-粉末床熔合工艺(LPBF)开发了一种原位合金化工艺,用于Fe-Cr-Co体系永磁材料的增材制造。这种新方法允许生产具有适合每种特定应用情况的化学成分的复杂合金,通过使用元素粉末或更简单的商业合金粉末作为基础材料来实现。本研究的核心重点是利用Fe-30.5Cr-15Co-1.5Mo合金开发和表征印刷工艺。通过对两种主要成分Fe和Cr粉末进行熔池试验,并使用两种不同成分球度的粉末混合物进行参数研究,开发了原位合金化工艺。选取样品,研究了不同印刷参数和印后处理对样品化学均匀性和磁性能的影响。此外,还进行了不同温度下的磁性测量,以研究3D打印材料磁性的温度稳定性。截至目前,磁性材料增材制造的研究数量还很低。大多数的研究都集中在含稀土磁性材料上。因此,在这项工作中,我们将采取另一个方向,我们将证明LPBF与原位合金化相结合是生产各种不同稀土自由磁性材料的理想方法。我们工作的积极结果可以对科学界产生影响,因为在不同有前途的稀土无磁性材料领域的进一步研究是值得期待的。此外,由于无稀土磁性材料的生产依赖于不同的原材料来源,因此可能会产生积极的经济影响,这些原材料来源既更具成本效益,又在供应链方面不那么重要。这种影响还伴随着积极的环境影响,因为稀土金属的开采通常会带来相当大的环境污染。
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