ISOLASI SELULOSA DARI SERAT SABUT KELAPA (Cocos nucifera L.) PADA VARIASI SUHU DAN WAKTU PROSES BLEACHING DENGAN ASAM PERASETAT

M. Santhi, I. W. Arnata, L. Wrasiati
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Abstract

Cellulose is a chemical component of lignocellulose that can be found in most cell walls and woody parts of plants. One of the plants that has a high cellulose content is coco fiber, which is 43.44%. However, the potential of cellulose content in coco fiber is still not optimally utilized. This study aims to determine the effect of the temperature and time of the bleaching process using peracetic acid (PA) on the characteristics of the cellulose produced, as well as to determine the best combination of temperature and time for the bleaching process with PA to produce coco fiber cellulose. This study used a randomized block design with two factors, that were temperature (60°C, 80°C, and 100°C) and time (30 minutes and 60 minutes). Data were analyzed by analysis of variance and continued with Duncan's multiple comparison test. Variables observed were yield, degree of whiteness, content of cellulose, hemicellulose, and lignin. The results showed that the treatment temperature and time of the bleaching process using PA had a significant effect on all observed variables. The interaction between temperature and time of the bleaching process had a significant effect on whiteness, cellulose, hemicellulose, and lignin content, but did not significantly affect the yield content of coco fiber. The best treatment to produce cellulose was obtained by using PA at a temperature of 100°C and a time of 60 minutes. The characteristics were 35.38±0.32% yield, 84.77±0.81% degree of whiteness, 83.14±0.22% cellulose, 6.60±0.51% hemicellulose, and 4.23±0.55% lignin.
从椰子纤维中分离纤维素(Cocos nucifera L)。温度和时间的变化与乳酸交替作用
纤维素是木质纤维素的一种化学成分,可以在大多数细胞壁和植物的木质部分中找到。可可纤维是纤维素含量高的植物之一,为43.44%。然而,椰子纤维中纤维素含量的潜力仍未得到充分利用。本研究旨在确定过氧乙酸(PA)漂白工艺的温度和时间对所制纤维素特性的影响,并确定PA漂白工艺的最佳温度和时间组合以生产可可纤维纤维素。本研究采用随机区组设计,温度(60°C、80°C和100°C)和时间(30分钟和60分钟)为两个因素。数据分析采用方差分析,继续采用Duncan多重比较检验。观察到的变量包括产量、白度、纤维素、半纤维素和木质素的含量。结果表明,PA漂白过程的处理温度和时间对所有观察变量都有显著影响。漂白温度和时间的交互作用对可可纤维的白度、纤维素、半纤维素和木质素含量有显著影响,但对可可纤维的得率没有显著影响。在温度为100℃,时间为60分钟的条件下,采用PA制备纤维素的最佳工艺。产率为35.38±0.32%,白度为84.77±0.81%,纤维素为83.14±0.22%,半纤维素为6.60±0.51%,木质素为4.23±0.55%。
本文章由计算机程序翻译,如有差异,请以英文原文为准。
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