Synthesis and Study of Thermo Physical Properties of Phthalic anhydride glycerol Resin (PAGR) from Soybean Oil

Shafqat Abbas, Zaheer Ahmad
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Abstract

Phthalic anhydride-glycerol Resin(PAGR) increase the flexibility of paint, resist to acid rain effect, increases the adhesiveness, brushing power, film hardness, layer flexibility, durability, gloss retention, resistance to abrasion also helps to decrease the overall drying time of paints. Phthalic anhydride-glycerol Resin is produced by reacting polyfunctional alcohol with the poly basic and monofunctional acid by Alcoholysis process. Moreover, Phthalic anhydride-glycerol Resin (PAGR) is a major raw material for coatings, varnishes and binders. Phthalic anhydride-glycerol Resin (PAGR) is used in paints coating compositions, adhesive, plastics, varnishes, printing ink, floor coverings. In the present research work, Phthalic anhydride-glycerol Resin is synthesized using soybean oil, pentaerythritol, phthalic anhydride and litharge (PbO). It was further characterized by FTIR, DSC TGA and acid value.
大豆油苯二酸酐甘油树脂(PAGR)的合成及热物理性能研究
邻苯二甲酸酐-甘油树脂(PAGR)增加油漆的柔韧性,抗酸雨效果,增加附着力,涂刷力,膜硬度,层柔韧性,耐久性,保光性,抗磨损性也有助于减少油漆的整体干燥时间。邻苯二酸酐-甘油树脂是由多官能团醇与多碱和单官能团酸用醇解法反应而成。此外,苯二酸酐-甘油树脂(PAGR)是涂料、清漆和粘合剂的主要原料。邻苯二甲酸酐甘油树脂(PAGR)用于油漆涂料组合物,粘合剂,塑料,清漆,油墨,地板覆盖物。本研究以大豆油、季戊四醇、邻苯二酸酐和邻苯二酸酐(PbO)为原料合成邻苯二酸酐-甘油树脂。并用FTIR、DSC、TGA和酸值对其进行了表征。
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