Green synthesis and characterization of iron nanoparticles from Bauhinia tomentosa

R. Devika
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Abstract

Introduction: Synthesis of metallic nanoparticles using plant extract is inexpensive, easily scaled up, and eco-friendly and their technique has wide open applications in various sectors such as medicine, health, and environment due to its mechanism of action for the betterment of human. The aforesaid challenges and principles of nanoparticles have advanced in the green synthesis utilizing the phytoconstituents to reduce and stabilize the metallic nanoparticles. Materials and Methods: In the investigation, green synthesis of iron nanoparticles from Bauhinia tomentosa was characterized under ultraviolet–visible spectrophotometer, Fourier transform infrared at various concentrations and durations. The characterized iron nanoparticles were analyzed for reducing assay and hydrogen peroxide assay to prove their antioxidant properties and antibacterial properties. Results and Discussion: When the plant extract was added to ferric chloride solution Fe3+ reduced to Fe0 which was indicated by the color change from green into blackish green proved the formation of iron nanomaterials (due to surface Plasmon resonance singularity). The synthesized iron nanomaterials were characterized by different parameters such as proportions (extract: Ferric chloride) and development study at different durations which are identified as factors affecting the yields of nanoparticles and later the nanoparticles were characterized. The reducing power of the iron nanoparticles synthesized from B. tomentosa was investigated by comparing with the reductive ability of ascorbic acid. Reducing power assay has proved to be one of the convenient and rapid screening method for measuring the antioxidant potential. Conclusion: In the present investigation, the plant bioactive constituents of B. tomentosa proved to be highly efficient as reducing agents, antibacterial agent which on further clinical investigation will prove to have high therapeutic value in the medical field.
毛毛紫荆铁纳米颗粒的绿色合成及表征
介绍:利用植物提取物合成金属纳米颗粒具有成本低廉、易于规模化、环境友好等优点,具有改善人类健康的作用机制,在医药、卫生、环境等领域有着广泛的应用前景。纳米颗粒的上述挑战和原理,推动了利用植物成分还原和稳定金属纳米颗粒的绿色合成。材料与方法:利用紫外-可见分光光度计和傅里叶变换红外光谱对毛毛紫荆绿色合成的铁纳米颗粒进行了表征。通过还原实验和过氧化氢实验对所制备的铁纳米粒子进行了分析,以证明其抗氧化和抗菌性能。结果与讨论:将植物提取物加入到氯化铁溶液中,Fe3+还原为Fe0,颜色由绿色变为墨绿色,证明了铁纳米材料的形成(由于表面等离子体共振奇异性)。通过配比(萃取物:氯化铁)和发育时间等参数对合成的铁纳米材料进行表征,确定了影响纳米颗粒产率的因素,并对纳米颗粒进行了表征。通过与抗坏血酸的还原能力进行比较,研究了绒毛白杆菌合成的铁纳米颗粒的还原能力。还原力法是一种简便、快速的测定抗氧化电位的筛选方法。结论:在本研究中,毛毛菌的植物活性成分被证明是高效的还原剂、抗菌药物,在进一步的临床研究中将证明其在医学领域具有很高的治疗价值。
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