Improved method for separation of silver nanoparticles synthesized using the Nyctanthes arbor-tristis shrub

Aakash Gupta, A. R. Koirala, Bikash Gupta, Niranjan Parajuli
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引用次数: 17

Abstract

Abstract Plant-mediated synthesis of silver nanoparticles through green chemistry approach has evolved into a new era of research; however, the heterogeneous size and dispersity of silver nanoparticles have limited its applications, such as surface-enhanced Raman scattering, plasmon resonance, and more specifically in the medical field of target drug delivery and therapeutic activity. Here-we investigated the effect of purification and separation modes on the dispersity, size, and morphology of silver nanoparticles, synthesized by plant extract (Nyctanthes arbor-tristis). Transmission electron microscopy revealed silver nanoparticles with an average diameter of 13.0 nm when synthesized through ethanol precipitation, which is advantageously smaller. This result suggests that the silver nanoparticles size can be fine-tuned by changing the separation mode during purification from plant extract. Due to uniformity, our obtained nanoparticles can be expected to show higher catalytic activity towards photochemical reactions, drug delivery and antibacterial activity due to the absence of inactive coating layer (capping agent).
利用夜荆灌木合成纳米银的改进分离方法
摘要植物介导合成纳米银的绿色化学方法已经发展成为一个新的研究方向;然而,银纳米颗粒的不均匀尺寸和分散性限制了其应用,如表面增强拉曼散射,等离子体共振,更具体地说,在靶药物递送和治疗活性的医学领域。在这里,我们研究了纯化和分离方式对植物提取物(Nyctanthes arbort -tristis)合成的银纳米粒子的分散性、大小和形态的影响。透射电镜显示,乙醇沉淀法合成的银纳米颗粒平均直径为13.0 nm,粒径较小。这一结果表明,在植物提取物的纯化过程中,可以通过改变分离模式来微调银纳米颗粒的大小。由于均匀性,我们获得的纳米颗粒可以预期在光化学反应,药物传递和抗菌活性方面表现出更高的催化活性,因为没有非活性涂层(封盖剂)。
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